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Analytical Data <br />Client: Kennedy/Jenks Consultants Job Number: 720-1310-1 <br />Client Sample ID: <br />Lab Sample ID:Date Sampled: <br />Date Received: <br />OU2-AOI7-S-4-0/1 <br />01/04/2006 0920 <br />01/04/2006 1745Client Matrix:Solid <br />8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) <br />720-1310-5 <br />Date Prepared: <br />Date Analyzed: <br />Dilution: <br />Preparation: <br />Method: <br />01/05/2006 1144 <br />01/06/2006 1613 <br />1.0 <br />8270C Analysis Batch: 720-4061 <br />Prep Batch: 720-3933 <br />Injection Volume: <br />Final Weight/Volume: <br />Initial Weight/Volume: <br />Lab File ID: <br />Instrument ID:Sat 2K2 <br />c:\saturnws\data\200601\01 <br />30.27 g <br />5 mL <br />3550B <br />Analyte Result (mg/Kg)RLQualifierDryWt Corrected: N <br />ND 0.844-Bromophenyl phenyl ether <br />ND 0.33Hexachlorobenzene <br />ND 1.6Pentachlorophenol <br />ND 0.33Phenanthrene <br />ND 0.33Anthracene <br />ND 0.84Di-n-butyl phthalate <br />ND 0.33Fluoranthene <br />ND 0.33Pyrene <br />ND 0.84Butyl benzyl phthalate <br />ND 0.843,3'-Dichlorobenzidine <br />ND 0.33Benzo[a]anthracene <br />ND 1.6Bis(2-ethylhexyl) phthalate <br />ND 0.33Chrysene <br />ND 0.84Di-n-octyl phthalate <br />ND 0.33Benzo[b]fluoranthene <br />ND 0.33Benzo[a]pyrene <br />ND 0.33Benzo[k]fluoranthene <br />ND *0.33Indeno[1,2,3-cd]pyrene <br />ND 0.33Benzo[g,h,i]perylene <br />ND 1.6Benzoic acid <br />ND 0.33Azobenzene <br />ND 3.3Dibenz(a,h)anthracene <br />Surrogate %Rec Acceptance Limits <br />83 23 - 120Nitrobenzene-d5 <br />95 30 - 1152-Fluorobiphenyl <br />112 18 - 137Terphenyl-d14 <br />88 25 - 1212-Fluorophenol <br />86 24 - 113Phenol-d5 <br />104 19 - 1222,4,6-Tribromophenol <br />STL San Francisco Page 41 of 186