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Quality Control Results <br />Job Number: 720-993-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/19/2005 1540 <br />12/19/2005 1609 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3184 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />12/16/2005 1549 <br />Prep Batch: 720-3184 <br />Analysis Batch: 720-3248 <br />c:\saturnws\data\200512\121905 <br />30.15 g <br />1 mL <br />c:\saturnws\data\200512\121905\ <br />30.18 g <br />1 mL <br />mg/Kg <br />12/16/2005 1549 <br />Analysis Batch: 720-3248 <br />Prep Batch: 720-3184 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K2 <br />Sat 2K2 <br />LCS 720-3184/2-A <br />LCSD 720-3184/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />8580 9 - 191 6 352,4-Dinitrophenol <br />98104 10 - 130 6 354-Nitrophenol <br />8481 10 - 130 3 35Dibenzofuran <br />9185 39 - 139 6 352,4-Dinitrotoluene <br />9190 50 - 158 1 352,6-Dinitrotoluene <br />8691 9 - 114 6 35Diethyl phthalate <br />8786 25 - 158 1 354-Chlorophenyl phenyl ether <br />8389 59 - 121 8 35Fluorene <br />8393 10 - 130 12 354-Nitroaniline <br />8787 9 - 181 0 352-Methyl-4,6-dinitrophenol <br />8883 10 - 130 6 35N-Nitrosodiphenylamine <br />8582 53 - 127 4 354-Bromophenyl phenyl ether <br />7481 9 - 152 9 35Hexachlorobenzene <br />8683 14 - 176 3 35Pentachlorophenol <br />8283 10 - 130 2 35Phenanthrene <br />8177 27 - 133 5 35Anthracene <br />8588 10 - 130 3 35Di-n-butyl phthalate <br />8082 26 - 137 3 35Fluoranthene <br />8282 52 - 115 0 35Pyrene <br />9094 10 - 130 4 35Butyl benzyl phthalate <br />6268 10 - 130 10 353,3'-Dichlorobenzidine <br />8284 33 - 143 3 35Benzo[a]anthracene <br />9397 8 - 158 4 35Bis(2-ethylhexyl) phthalate <br />8185 17 - 168 4 35Chrysene <br />8285 4 - 146 4 35Di-n-octyl phthalate <br />8584 24 - 159 0 35Benzo[b]fluoranthene <br />8888 17 - 163 0 35Benzo[a]pyrene <br />8484 11 - 162 1 35Benzo[k]fluoranthene <br />830 9 - 171 200 35 **Indeno[1,2,3-cd]pyrene <br />8385 9 - 219 3 35Benzo[g,h,i]perylene <br />2829 10 - 130 5 35Benzoic acid <br />8186 10 - 130 5 35Azobenzene <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 117 of 141