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Quality Control Results <br />Job Number: 720-993-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/16/2005 1339 <br />12/16/2005 1343 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3130 <br />1.0 <br />1.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3150 <br />Analysis Batch: 720-3150 <br />12/16/2005 0619 <br />12/16/2005 0619 <br />Prep Batch: 720-3130 <br />Prep Batch: 720-3130 <br />1.01 g <br />50 mL <br />1.00 g <br />50 mL <br />Method: 6010B <br />Preparation: 3050B <br />N/A <br />N/A <br />Varian ICP <br />Varian ICP <br />720-993-10 <br />720-993-10 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />38 42 75 - 125 9 20 **Antimony <br />88 111 75 - 125 21 20 *Arsenic <br />72 93 75 - 125 9 20 *Barium <br />81 83 75 - 125 3 20Beryllium <br />79 84 75 - 125 6 20Cadmium <br />84 89 75 - 125 4 20Chromium <br />79 83 75 - 125 5 20Cobalt <br />81 132 75 - 125 17 20 *Copper <br />101 100 75 - 125 0 20Lead <br />88 90 75 - 125 3 20Molybdenum <br />77 83 75 - 125 4 20Nickel <br />78 74 75 - 125 4 20 *Selenium <br />94 98 75 - 125 5 20Silver <br />79 81 75 - 125 3 20Thallium <br />90 84 75 - 125 5 20Vanadium <br />73 72 75 - 125 0 20 **Zinc <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 131 of 141