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MA N A L Y T I C A L LABORATORIES Casey Weaver Certificate of Analysis BSK & Associates - Sacramento Report Issue Date 04/17/2000 3140 Gold Camp Drive Suite 160 ' Rancho Cordova, CA 95670 BSK Submission#: 2000040046 BSK Sample ID #: 33414 Project lD 07400178 Project Desc. Greer Submission Comments Sample Type Liquid Date Sampled. 04/03/2000 Sample Description W-67-MW4 Time Sampled. 1014 ' Sample Comments Date Received. 04/04/2000 Olreanics Prep Analyses Analvte Method Result Units PQL Dduteon DLR Date Date TPH as Gasolme EPA 8015M 350 lig/L 50 1 50 04/12/2000 04/12/2000 Benzene EPA 8020 59 µg/L 0 3 1 0 3 04/12/2000 04/12/2000 Ethylbeame EPA 8020 ND µg/L 0 3 1 0 3 04/12/2000 04/12/2000 Toluene EPA 8020 0.44 µg/L 0 3 1 0 3 04/12/2000 04/12/2000 Total Xylenes EPA 80220 39 µg/L 0 3 1 0 3 04/12/2000 04/12/2000 1,2-Dibromoethane EPA 8260 ND µg/L 50 1 5 04/1012000 04/10/2000 1,2-Dichloroethane EPA 8260 ND AWL 50 1 5 04/I0/2000 04/10/2000 Di-isopropyl Ether EPA$260 ND µg/L 5 0 1 5 04/10/2000 04/10/2000 Ethyl t-Butyl Ether EPA 8260 ND lig/L 50 1 5 04/10/2000 04/10/2000 Methyl-t Butyl Ether EPA 8260 ND lig(L 50 1 5 0 04/10/2000 04/10/2000 t Amyl Methyl Ether EPA 8260 ND lig/L 5 0 1 5 04/10/2000 04/10/2000 tort Butyl Alcohol EPA 8260 ND pg/L 50 1 50 04/10/2000 04/10/2000 ' LUF F Comments TPH as Gasoline Higher boilmg point hydrocarbons decreased relative to standard 1 ' ml~/L milligmins/liter(ppm) PQL practical quantitation limit H analyzed outside of hold time . mg/Kg nulligmms/lalogram(ppm) DLR. detection limit for reporting P preliminary result ' pg/L micrograms/liter(ppb) PQL x Dilution S suspect result pg/Kg microgramwWogram(ppb) ND none detected at DLR %Ree percent recovered(surrogates) ' 1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935