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Amei K an E11171 onniewal Network WORK ORDER 9709281 QUALITY CONTROL REPORT PAGE QR-4 1 ANALYSIS Metals Scan by ICP ' MATRIX: Water METHOD BLANK SAMPLES SAMPLE TYPE Blank-Method/Media blank LAB ID IFW BLNK T INSTR RUN ICP1970930134000/l/ INSTRUMENT TJA Enviro 36 PREPARED 09/27/9T- BATCH ID IFW092797 T UNITS mg/L ANALYZED 09/30/97 DILUTION 1 000000 ' METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (%) LOW HIGH RPD (X) LIMIT (X) Fe Iron NO 0 1 LABORATORY CONTROL SAMPLES SAMPLE TYPE Spike-Method/Media blank LAB ID IFW LCD T INSTR RUN ICP1970930134000/3/1 INSTRUMENT TJA Enviro 36 PREPARED 09/27/97 BATCH ID IFW092797 T UNITS mg/L ANALYZED 09/30/97 DILUTION 1 000000 METHOD ' REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) Fe Iron 0 529 NO 0 1 0 500 106 84 133 -- - -- --- - - --- - - - - -- - - - -- - -- - -- - --- - - - ------- - - - - -- --- -- ---- - - - - ' SAMPLE TYPE Spike Method/Media blank LAB ID IFW LCS T INSTR RUN ICP1970930134000/2/1 INSTRUMENT TJA Enviro 36 PREPARED 09/27/97 BATCH ID IFW092797 T UNITS mg/L ANALYZED 09/30/97 DILUTION 1 000000 METHOD • REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) Fe Iron 0 516 ND 0 1 0 500 103 84 133 -- -- - -- - - - --- --- -- --- -- - - - -- - -- - -- -- - - ---- - - - - --- ----- - ---- - - LABORATORY CONTROL DUPLICATES SAMPLE TYPE Method Spike Sample Duplicate LAB ID IFW LCR T INSTR RUN ICP1970930134000/4/2 INSTRUMENT TJA Enviro 36 PREPARED 09/27/97 BATCH ID IFW092797 T UNITS mg/L ANALYZED 09/30/97 DILUTION 1 000000 METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) Fe Iron 0 529 0 516 0 1 2 49 10 •