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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 <br /> Job Number: C25653 <br /> Account: KFCAI Kleinfelder, Inc.-Irvine <br /> Project: Costco-Lodi, CA <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> C25653-3MS L21826.D 1 01/10/13 XB n/a n/a VL693 <br /> C25653-3MSD L21827.D 1 01/10/13 XB n/a n/a VL693 <br /> C25653-3 L21824.D 1 01/10/13 XB n/a n/a VL693 <br /> as <br /> The QC reported here applies to the following samples: Method: SW846 8260B -+ <br /> C25653-1, C25653-2, C25653-3 <br /> C25653-3 Spike MS MS MSD MSD Limits <br /> CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD <br /> 71-43-2 Benzene ND 39.7 45.2 114 42.7 108 6 81-119/20 <br /> 100-41-4 Ethylbenzene ND 39.7 43.3 109 40.8 103 6 80-119/21 <br /> 1634-04-4 Methyl Tert Butyl Ether ND 39.7 49.3 124 45.5 115 8 79-127/19 <br /> 108-88-3 Toluene ND 39.7 42.7 108 40.5 102 5 80-117/21 <br /> 1330-20-7 Xylene(total) ND 119 128 108 120 101 6 81-122/22 <br /> CAS No. Surrogate Recoveries MS MSD C25653-3 Limits <br /> 1868-53-7 Dibromofluoromethane 110% 105% 108% 71-125% <br /> 2037-26-5 Toluene-138 105% 106% 108% 82-121% <br /> 460-00-4 4-Bromofluorobenzene 100% 100% 99% 80-120% <br /> * = Outside of Control Limits. <br /> so 17 of 17 <br /> v ACCUTEST. <br /> C25653 <br />