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110 2nd Avenue South,#177,Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925 798-1620 Fax 925-798-1622 <br /> httpJlwww TricLarripbell cam E-mail rnain@mccampbell com <br /> Advanced GeoEnvironmental, Inc Client Protect TD Langston's Market Date Sampled 09/08/03 <br /> 837 Shaw Road Date Received 09/09/03 - <br /> rClient Contact Paul Dotson Date Extracted 09/11/03 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 09/11/03 <br />' Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0309139 <br /> Lab ID 0309139-005B 10309139-006B 0309139-007B--0309139-008B <br /> Client ID MW5/080903 MW6/080903 MW7/080903 MW8/080903 <br /> Reporting Limit for <br /> Matrix -W __—W _--__----W - W DF=l <br /> —A <br /> ::D:F]- 5 1 1 1 S W <br /> _F_ <br /> Compound Concentration ug/kg µg/L <br /> tent-Amyl methyl ether(TAME) ND<2 5 ND ND ND NA 05 <br />' Benzene 6 l ND ND ND NA 0 5 <br /> t-Butyl alcohol('CBA) ND<25 ND ND ND NA 5 0 <br /> 1,2-Dibrornoethane(EDB) ND<2 5 ND ND ND NA 0 5 <br /> 1,2-Dichloroethane(1,2-DCA) ND<2 5 ND ND ND NA 0 5 <br /> Dusopropyl ether(DIPE) ND<2 5 ND ND ND NA 0 5 <br /> Ethylbenzene 78 ND ND ND NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND<2 5 ND ! ND ND NA 0 5 <br />' Methyl-t-butyl ether(MTBE) 40 ND i ND ND NA 0 5 <br /> Toluene ND<2 5 ND ND ND NA 0 5 <br />' Xylenes ND<2 5 ND ND ND NA 0 5 <br /> Surrogate Recoveries{%) <br />' %SS1 962 992 988 99 7 <br /> %SS2 100 105 105 105 <br /> 1 %SS3 875 83 7 780 82 6 <br />' Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported to gg/L,soil/sludge/solid samples 1n 14g/kg, wipe samples in pg/wtpe <br /> product oil/non-aqueous liquid samples in mg/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br />' h)lighter than water immiscible sheen/product is present i)liquid sample that contains greater than-2 vol %sediment,a)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 _Angela Rydelius, Lab Manager <br /> 1 <br />