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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccamT)bell.com E-mail: main@mccampbell.com <br /> Upgradient Environmental Client Project ID: #99027.2;Stockton Date Sampled: 08/24/99 <br /> Terminal&Eastern Railroad Date Received: 08/25/99 <br /> 336 Augusta Court <br /> Valley Springs,CA 95252 Client Contact:Vic Cherven Date Extracted: 08/25/99 <br /> Client P.O: Date Analyzed:08125-09101199 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel* <br /> EPA methods modified 8015,and 3550 or 3510:California RW B SF Bav Reeionl method GCFID(3550)or CrCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)- %Recovery <br /> Surrogate <br /> 17885 BI-15' S 8500,a 101 <br /> 17886 B1-20' S 9100,a 107 <br /> 17887 131-25' S ND 101 <br /> 17888 B1-30' S ND 108 <br /> 17890 B1-40' S ND 102 <br /> 17892 132-15' S ND 108 <br /> 17893 132-20' S ND 108 <br /> 17895 132-30' S ND 108 <br /> 17896 133-W W 1,700,000,g,a 95 <br /> 17899 134-15' S ND 101 <br /> 17900 B4-20' S ND 100 <br /> 17902 134-30S ND 99 <br /> 17904 B5-15' S ND 99 <br /> 17905 135-20' S ND 99 <br /> 17907 B5-30' S ND 98 <br /> Reporting Limit unless otherwise W 50 ug(L <br /> stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg <br /> *water and vapor samples are reported in ug/L,wipe samples in uglwipe,soil and sludge samples in mg/kg,and all TCLP I STLC I SPLP <br /> extracts in ug/L <br /> "cluttered chromatogram resulting in coeluted surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(?);f) <br /> one to a few isolated peaks present; g) oil range compounds are significant; h) lighter than water immiscible sheen is present; i) liquid <br /> sample that contains greater than—5 vol.%sediment. <br /> DHS Certification No. 1644 JQ-L, Edward Hamilton,Lab Director <br />