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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Results <br /> Client Applied Earth-Sciences, Inc Service-Request.—X2400480 <br /> Project Canteen Corp Date Collected 05/13/2004 <br /> On ple Matrix Water Date Received 05/14/2004 <br /> IVolatile Organic Compounds <br /> Sample Name MW 13 Units ug/L <br /> Lab Code X2400480-005 Basis NA <br /> Extraction Method EPA 5030B Level Low <br /> Analysis Method 8260B <br /> Dilution Date Date Extraction <br /> Analyte Name _ Result Q MRL MDL Factor Extracted Analyzed Lot Note <br /> Methyl tent-Butyl Ether 1500 D 500 400 500 05/20/04 05/20/04 XWC0400570 <br /> Benzene 14000 D 250 150 500 05/20/04 05/20/04 XWG0400570 <br /> 1,2-D,chloroethane ND U 250 250 500 05/20/04 05/20/04 XWG0400570 <br /> Toluene 22000 D 250 100 500 05/20/04 05/20/04 XWG0400570 <br /> 1,2-Dibromoetliane ND U 250 150 500 05/20/04 05/20/04 XWG0400570 <br /> Ethylbenzeoe 1400 D 250 100 500 05/20/04 05/20/04 XWG0400570 <br /> m,p-Xylenes 9800 D 500 300 500 05/20/04 05/20/04 XWG0400570 <br /> o-Xylene 4700 D 250 150 500 05/20/04 05/20/04 XWG0400570 <br /> tert-Butyl Alcohol ND U 10000 5000 500 05/20/04 05/20/04 XWG0400570 <br /> Diisopropyl Ether ND U 500 200 500 05/20/04 05/20/04 XWG0400570 <br /> tert-Amy]Methyl Ether ND U 250 150 500 05/20/04 05/20/04 XWG0400570 <br /> tert-Butyl Ethyl Ether ND U 250 150 500 05/20/04 05/20/04 XWG0400570 <br /> 10 <br /> IControl Date <br /> Surrogate Name %Rec Limits Analyzed Note <br /> Dibromofluoromethane 107 77-121 05/20/04 Acceptable <br /> IToluene-d8 108 65-131 05/20/04 Acceptable <br /> 4-Bromofluorobenzene 104 68-125 05/20/04 Acceptable <br /> I <br /> I <br /> OrnLnts <br /> Printed 09/29/2004 0116 50 Form IA-Organic Page 1 of 1 <br /> L 1STEALMCRYSTAL RPTNFormlm rpt Merged SuperSet Reference RR4622 <br />