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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Results <br /> Chent Apphed Earth Sciences,Inc Service Request L2400548 <br /> Protect Canteen Corp/AGE-NC-99-0612 Date Collected 02/24/2004 <br /> �ple Matrix Water Date Received 02/26/2004 <br /> IVolatile Organic Compounds <br /> Sample Name MW3D/022404 Units ug/L <br /> Lab Code L2400548-003 Basis NA <br /> Extraction Method, EPA 5030B Level Low <br /> IAnalysis Method 8260B <br /> Dilution Date Date Extraction <br /> IAnalyte Name Result Q PQL MDL Factor Extracted Analyzed Lot Note <br /> Benzene 2 9 050 0 19 1 03/08/04 03/08/04 LWG0401005 <br /> 1,2-Dibromoethane (EDB) ND U 050 0 17 1 03/08/04 03/08/04 LWG0401005 <br /> I1,2-Dichloroethane(EDC) ND U 050 024 1 03/08/04 03/08/04 LWG0401005 <br /> EthyIbenzene 6 0 050 0 18 1 03/08/04 03/08/04 LWG0401005 <br /> Toluene ND U 050 0 17 1 03/08/04 03/08/04 LWG0401005 <br /> 0-Xylene ND U 050 0 13 1 03/08/04 03/08/04 LWG0401005 <br /> m,p-Xylenes 041 J 1 0 027 1 03/08/04 03/08/04 LW60401005 <br /> Dnsopropyl Ether ND U 2 0 035 1 03/08/04 03/08/04 LWG0401005 <br /> tert-Butyl Ethyl Ether ND U 2 0 028 1 03/08/04 03/08/04 LWG0401005 <br /> tert-Amyl Methyl Ether ND U 2 0 032 1 03/08/04 03/08/04 LWG0401005 <br /> Methyl tert-Butyl Ether 8 6 1 0 031 1 03/08/04 03/08/04 LWG0401005 <br /> -Butyl Alcohol ND U 20 3 3 1 03/08/04 03/08/04 LWG0401005 <br /> Control Date <br /> Surrogate Name %Rec Limits Analyzed Note <br /> Dibromofluoromethane 118 72-134 03/08/04 Acceptable <br /> Toluene-d8 106 82-118 03/08/04 Acceptable <br /> 4-Bromofluorobenzene 93 71-119 03/08/04 Acceptable <br /> I <br /> I <br /> omments <br /> 7 <br /> IPrinted 03/12/2004 15 48 00 Form IA-Organic Page 1 of 1 <br /> P 1STFAL"fH1CRYSTAL RPTSF,rm1 m rpt Merged SuperSet Reference RR5281 <br />