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' 1102nd AVC11MSuu111 IS07 PILlileo CA 94 53 »60 <br /> M Campbell Analytical Inc relephoue 92� 796 1620 Fax 92a 79M 1022 <br /> 111tp/rwww111ccaritpbeli40111 £mail ilia]tp;tnc,aui:,bellCow <br /> QC SUMMARY REPORT FOR SW8260B <br /> Matrix W Work rder 0308200 <br /> EPA Method SW8260B Extraction SW5030B BatchlD 8169 Spiked Sample ID 308193-0108 <br /> Sample Spiked MS' f MSD' MS-MSD" LCS I.CSD rLCS LCSD Acce Lance Criteria M <br /> tiglL pglL % Rec ! % Rec I % RPD % Rec i % Rec T % RPD l ow High <br /> teit Amyl meshy!ethei (1 AML) ND 10 925 92 9 0 395 109 101 8 38 711 130 <br /> t-Butyl dlLohol(I 13A) ND 50 932 9.) 2 2 13 114 103 102 71 130 <br /> 1 2 Dibromoetltane(EDB) ND 10 T105 108 2 78 122 113 729 70 130 <br /> 1 2-DtchloiWhine(I,2-DCA) NI) 10 110 112 1 89 129 120 7 36 7 130 <br /> Dnsopropyl ether(D1PE) ND 10 - 114--- <br /> l l7 2 62 104 120 179 70 130 <br /> Ethyl Lei t-butyl ether (E rBE) ND 10 98 5 100 l 78 117 107 935 7 130 <br /> Methyi-t-butyl ether (M I BE) ND 10 996 - 101 2 73 115 105 8 65 7t. 130 <br /> 119W 100 108 T 110 179 t 98 I 102- T 3 57W-- - - 7 -- j� 130 <br /> Ali target compounds in 111L Method Blanket(]its extraction hatch were ND less than the method RL with the following exccpuons <br /> NONE <br /> MS=Matrix Spike MSD w Matrix Spike Duplicate LCS=LaboratoryControl Sample LCSD=LaboratoryControl Sample Dupiicale RPD=Reative Percent <br /> Deviation <br /> %Recovery= 100 (MS Sample);(Amount Spiked) RPD= 100 (MS-MSD)I(MS r MSD) 2 <br /> MS and/or MSD spike recoveries may not be near 100%or We RPDs near 0%if i)the sampie rs inhomogenous AND contains significant icncentralions c' <br /> analyte relative to the amount spiked or b)if that specific sample matrix interferes with spike recovery <br /> N =not enough sample to perform matrix spike and matrix spike dupElcate <br /> R=analyte concentration m sample exceeds spike amount for sod matrix or exceeds 2x spike amount for water mainx or sample diluted duet high matrix or <br /> analyte t.ontent <br /> Laboratory extraction solvents such as methylene chloride and acetone may occasionsily appear in the method blank al Sow ieveis <br />