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110 2nd Avenue South,#137 Pacheco CA 94553-3560 <br /> LAA—McCampbell Analytical Inc Telephone 925-798 1620 Fax 925 798 1622 <br /> http/Iwwwtnccatmbellcom Email mam Mmccampbell com <br /> A E S Regulatory Services Client Project ID Canteen Corp Date Sampled 05/27/03 <br /> 2013 Wells Branch Pkwy Ste 206 Date Received 05/28/03 <br /> Client Contact Paul Dotson Date Extracted 05/29/03-05/30/03 <br /> Austin, TX 78728 <br /> Client P O Date Analyzed 05/29/03-05/30/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0305421 <br /> Lab ID 0305421-005B 0305421-006B 0305421-007B <br /> Client ID MW 13 MW 13A MW 13B <br /> Reporting Limit for <br /> Matrix W W W DF=1 <br /> DF 1000 - -1 S W <br /> Compound ancentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND<500 f� ND ND NA I 05 <br /> Benzene 29,000 E 0 84 ND NA I 0 5 <br /> t-Butyl alcohol(TBA) ND<5000 f ND ND NA 5 0 <br /> 1 2-Dibromoethane(EDB) ND<500 ND ND NA 0 5 <br /> 12-Dichloroethane(1,2-DCA) ND<500 ND ND NA 0 5 <br /> Drtsopropyl ether(DIPS) ND<500 i ND ND NA 0 5 <br /> • Ethylbenzene 3000 I 3 2 ND NA 0 5 <br /> i <br /> Ethyl tert-butyl ether(ETBE) ND<500 ND ND NA I 0 5 <br /> Methyl t-butyl ether(MTBE) 1600 ND ND NA 0 5 <br /> Toluene 42,000 2 3 ND NA O 5 <br /> Xylenes 24,000 8 0 ND NA I 0 5 <br /> Surrogate Recoveries (%) <br /> �T%5S1 - - 94 3- � 95 9 — 965 <br /> %SS2 999 997 102 <br /> %SS3 101 968 107 <br /> Comments {{ <br /> � f <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in ltg/L,soil/sludge/solid samples in gg/kg, wipe samples inµg/wipe, <br /> productloil/nun-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />