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Report Number: 31338 QC Report : Method Blank Data Date : 02/21/2003 Project Name : Delta # 4509-T Project Number: Method Method Parameter Limit Measured Reporting Analysis Date Measured Reporting Analysis Date Value Units Method Analyzed Parameter Value Limit Units Method Analyzed TPH as Diesel <1.0 1.0 mg/Kg M EPA 8015 02/11/2003 Benzene <0.0050 0.0050 mg/Kg EPA 82608 02/13/2003 1-Chloroocladecane(Diesel Surrogate) 106 % M EPA 8015 02/11/2003 Toluene <0.0050 0.0050 mg/Kg EPA 82608 02/13/2003 Ethylbenzene <0.0050 0.0050 mg/Kg EPA 8260B 02/13/2003 TPH as Diesel <50 50 ug/L M EPA 8015 02/09/2003 Total Xylenes <0.0050 0.0050 mg/Kg EPA 8260B 02/13/2003 Methyl-t-butyl ether(MTBE) <0.0050 0.0050 mg/Kg EPA 82608 02/13/2003 Benzene <0.0050 0.0050 mg/Kg EPA 8260B 02/11/2003 Diisopropyl ether DIPE < Toluene (DIPE) 0.0050 0.0050 mg/Kg EPA 8260B 02/13/2003 <0.0050 0.0050 mg/Kg EPA 82608 02/11/2003 Ethyl-t-butyl ether(ETBE) <0.0050 0.0050 mg/Kg EPA 8260B 02/13/2003 Ethylbenzene <0.0050 0.0050 mg/Kg EPA 8260B 02/11/2003 Tert-am I methyl ether TAME < Total Xylenes <0.0050 0.0050 mg/Kg EPA 8260B 02/11/2003 y y (TAME) 0.0050 0.0050 mg/Kg EPA 8260B 02/13/2003 Tart-Butanol <0.0050 0.0050 mg/Kg EPA 82608 02/13/2003 Methyl-t-butyl ether(MTBE) <0.0050 0.0050 mg/Kg EPA 82608 02/11/2003 Methanol <0.20 0.20 mg/Kg EPA 82608 02/13/2003 Diisopropyl ether(DIPE) <0.0050 0.0050 mg/Kg EPA 8260B 02/11/2003 Ethanol <0.010 0.010 mg/Kg EPA 8260B 02/13/2003 Ethyl-t-butyl ether(ETBE) <0.0050 0.0050 mg/Kg EPA 8260B 02/11/2003 TPH as Gasoline < Tert-amyl methyl ether(TAME) <0.0050 0.0050 mg/Kg EPA 8260B 02/11/2003 1.0 1.0 mg/Kg EPA 8260B 02/13/2003 1,2-Dichloroethane <0.0050 0.0050 mg/Kg EPA 82608 02/13/2003 Tert-Butanol 0.0068 0.0050 mg/Kg EPA 8260B 02/11/2003 Methanol <0.20 0.20 mg/Kg EPA 8260B 02/11/2003 1,2-Dibromoethane <0.0050 0.0050 mg/Kg EPA 82608 02/13/2003 Ethanol <0.010 0.010 mg/Kg EPA 82608 02/11/2003 Toluene-d8(Surr) 97.2 % EPA 8260B 02/13/2003 TPH as Ga:;oline <1.0 1.0 mg/Kg EPA 8260B 02/11/2003 4-Bromofluorobenzene(Surr) 104 % EPA 8260B 02/13/2003 Dibromofluoromethane(Surr) 102 % EPA 82608 02/13/2003 1,2-Dichloroethane <0.0050 0.0050 mg/Kg EPA 8260B 02/11/2003 1,2-Dichloroethane-d4(Surr) 105 1,2-Dibromoetliane <0.0050 0.0050 mg/Kg EPA 8260B 02/11/2003 % EPA 82608 02/13/2003 Toluene-da(Surr) 100 % EPA 8260B 02/11/2003 Benzene <0.50 0.50 ug/L EPA 8260B 02/10/2003 4-Bromofluorobenzene(Surr) 101 % EPA 82606 02/11/2003 Toluene <0.50 0.50 ug/L EPA 8260B 02/10/2003 Dibromofluoromethane(Surr) 102 % EPA 8260B 02/11/2003 Ethylbenzene <0.50 0.50 ug/L EPA 8260B 02/10/2003 1,2-Dichloroethonerl4(Surr) 105 % EPA 8260B 02/11/2003 Total Xylenes <0.50 0.50 ug/L EPA 82608 02/10/2003 Methyl-t-butyl ether(MTBE) <0.50 0.50 ug/L EPA 8260B 02/10/2003 Diisopropyl ether(DIPE) <0.50 0.50 ug/L EPA 8260B 02/10/2003 Ethyl-t-butyl ether(ETBE) <0.50 0.50 ug/L EPA 82608 02/10/2003 Tert-amyl methyl ether(TAME) <0.50 0.50 ug/L EPA 8260B 02/10/2003 Tert-Butanol <5.0 5.0 ug/L EPA 8260B 02/10/2003 Methanol <50 50 ug/L EPA 8260B 02/10/2003 Ethanol <5.0 5.0 ug/L EPA 8260B 02/10/2003 1,2-Dichloroethane <0.50 0.50 ug/L EPA 8260B 02/10/2003 1,2-Dibromoethane <0.50 0.50 ug/L EPA 8260B 02/10/2003 TPH as Gasoline <50 50 ug/L EPA 8260B 02/10/2003 Toluene-d8(Surr) 104 % EPA 8260B 02/10/2003 KIFF ANALYTICAL, LLC Approved By: JI of l Kiff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800 V