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r <br />'ff Geonalytical Laboratoriesnc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS . <br /> Repan°# N100-11 Oxygenates Date: 4/15/02 ' <br /> Thorpe Oil <br /> Project: Stockton Fire Station-Sonora St. Date Recd: 4/10/02 <br /> PO Box 357 Date Started: 4/11/02 <br /> Lodi CA 95241 PO# Date Completed:4/11/02 <br /> Date Sampled: 4/10/02 <br /> Sampler: R.Chrun/R.Azevedo <br /> Sample ID Lala ID RL Method Analyte Results Units <br /> Soil Sample#1 South451/2' N200874 10 8260B Methyl tert-butyl ether(MTBE) ND /Kg <br /> 400 Ethanol ND <br /> >lg <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPS) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% I' <br /> 1,2-Dichloroethane-d4 20 20.3 101.5 66-133 <br /> 2-Bromo-1-chloropropane 20 20.2 101 63-139 <br /> 4-Bromofluorobenzene 20 17,9 89.5 64-136 <br /> Soil Sample#2 South@4'" N200875 500 8260B Methyl tert-butyl ether (MTBE) ND pg/Kg <br /> 20000 Ethanol ND <br /> 10000 tert-Butanol ND <br /> 500 di-Isopropyl ether(DIPE) ND <br /> 500 Ethyl tert-butyl ether(ETBE) ND <br /> 500 tert-Amyl methyl ether(TAME) ND . <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit96 <br /> 1,2-Dichloroethane-d4 5000 5710 114.2 66-133 <br /> 2-Bromo-l-chloropropane 5000 5360 107.2 63-139 <br /> 4-Bromofluorobenzene 5000 5210 104.2 64-136 <br /> Elevated detection limits due to high level of non-target analytes. <br /> Soil Sample 43 South04' N200876 10 8260B Methyl tert-butyl ether(MTBE) ND pg/Kg <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether{DIPE) ND <br /> 10 Ethyl tert-butyl ether (ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit <br /> 1,2-Dichloroethane-d4 20 18.2 91 66-133 <br /> 2-Bromo-1-chloropropane 20 19.1 95.5 63-139 <br /> 4-Bromofluorobenzene 20 17.2 86 64-136 <br /> � l <br /> 'Mario D'Onofri Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />