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1 ! <br /> Eizv1/onmG;Lrc�� <br /> j t x <br /> ♦1 <br /> WORK ORDER 9712009 QUALITY CONTROL REPORT PAGE QR-2 <br /> ANALYSIS Gasoline Oxygenates <br /> MATRIX Water <br /> METHOD BLANK SAMPLES <br /> SAMPLE TYPE Blank Method/Media blank LAB ID BLNK 1205 INSTR RUN GCMS12\971205000000/1/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED — BATCH ID MS12WI20697 <br /> UNITS ug/L ANALYZED 12/05/97 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> - 1,2 DCE d4 (surr) 101 100 100 101 70 130 <br /> Toluene d8 (surr) 99 0 100 100 99 0 70 130 <br /> Bromofluorobenzene (surr) 96 5 100 100 96 5 70 130 <br /> Methy t butyl ether (MTBE) ND 5 <br /> Ethyl t butyl ether (ETRE) ND 5 <br /> t Amylmethyl ether (TAME) NO 5 <br /> t Butanol (TBA) NO 100 <br /> Di isopropyl ether (RIPE) ND 5 <br /> LABORATORY CONTROL SAMPLES <br /> --- - - - - - -- --- - - - - - --- - -- - - -- -- - - <br /> SAMPLE TYPE Laboratory Control Spike LAB ID LC5 1206 INSTR RUN GCMS12\971205000000/7/1 <br /> INSTRUMENT HP mass spec for Volatiles PREPARED — BATCH ID MS12W120697 <br /> UNITS ug/L. ANALYZED 12/06/97 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCE d4 (surr) 112 101 100 100 112 70 130 <br /> Toluene-d8 (surr) 102 99 0 100 100 102 70 130 <br /> Bromofluorobenzene (surr) 98 3 96 5 100 100 98 3 70 130 <br /> Methy t butyl ether (MTBE) 140 NO 5 100 140 32 158 <br /> Ethyl t-butyl ether (ETBE) 147 ND 5 100 147 32 158 <br /> t Amylmethyl ether (TAME) 130 ND 5 100 130 32 158 <br /> SAMPLE SURROGATES <br /> SAMPLE TYPE Sample Client LAB ID 9712009 01C INSTR RUN GCMS12\971205000000/9/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12W120697 <br /> UNITS ug/L ANALYZED 12/06/97 DILUTION 10 0 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCE d4 (surr) 108 1000 100 108 70 130 <br /> Toluene d8 (surr) 100 1000 100 100 70 130 <br /> Bromofluorobenzene (surr) 99 0 1000 100 99 0 70 130 <br /> SAMPLE TYPE Sample Client LAB ID. 9712009 02C INSTR RUN GCMS12\971205000000/10/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12W120697 <br /> UNITS ug/L. ANALYZED 12/06/97 DILUTION 10 0 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1,2 DCE d4 (surr) 114 1000 100 114 70 130 <br /> Toluene d8 (surr) 99 0 1000 100 99 0 70 130 <br /> Bromofluorobenzene (surr) 101 1000 100 101 70 130 <br /> SAMPLE TYPE Sample Client LAB ID 9712009 03C INSTR RUN GCMS12\971205000000/11/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12W120697 <br /> UNITS ug/L ANALYZED 12/06/97 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (1) LIMIT (X) <br /> 1 2-DCE d4 (surr) 102 100 100 102 70 130 <br /> Toluene d8 (surr) 99 1 100 100 99 1 70 130 <br /> Bromofluorobenzene (surr) 96 0 100 100 96 0 70 130 <br />