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11 � <br /> Al-11e, is iii iv o iCei7ta1 NEi`bi n <br /> R1 � <br /> WORK ORDER 9712009 QUALITY CONTROL REPORT PAGE QR-4 <br /> ANALYSIS TPH as Diesel <br /> MATRIX Water <br /> METHOD BLANK SAMPLES <br /> SAMPLE TYPE Blank Method/Media blank LAB ID BLNK 1205 2 INSTR RUN GC C1971205000000/25/ <br /> INSTRUMENT HP 5890 PREPARED 12/05/97 BATCH ID DSEW120597 2 <br /> UNITS mg/L ANALYZED 12/09/97 DILUTION 1 000000 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> r Diesel ND 0 05 <br /> Motor Oil ND 0 2 <br /> n Pentacosane (surr) 110 100 65 125 <br /> LABORATORY CONTROL SAMPLES <br /> - - - -- - - - - -- -- -- - - - -- -- - -- - - - ---- -- - - <br /> SAMPLE TYPE Laboratory Control Spike LAB ID LCDW 1205 2 INSTR RUN GC C1971205000000/27/25 <br /> INSTRUMENT HP 5890 PREPARED 12/05/97 BATCH ID DSEW120597 2 <br /> UNITS mg/L ANALYZED 12/09/97 DILUTION 1 000000 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> Diesel 2 19 NO 0 05 2 00 110 60 110 <br /> n Pentacosane (surr) 111 110 100 111 65 125 <br /> SAMPLE TYPE Laboratory Control Spike LAB ID LCSW 1205 2 INSTR RUN GC C1971205000000/26/25 <br /> INSTRUMENT HP 5890 PREPARED 12/05/97 BATCH ID DSCW120597 2 <br /> UNITS mg/L ANALYZED 12/09/97 DILUTION 1 000000 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (%) <br /> Diesel 2 19 ND 0 05 2 00 110 60 110 <br /> n Pentacosane (surr) 113 110 100 113 65 125 <br /> LABORATORY CONTROL DUPLICATES <br /> SAMPLE TYPE Laboratory Control Sample Duplicate LAB ID LCRW 1205 2 INSTR RUN GC C1971205000000/28/26 <br /> INSTRUMENT HP 5890 PREPARED 12/05/97 BATCH ID DS04120597 2 <br /> UNITS mg/L ANALYZED 12/09/97 DILUTION 1 000000 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (%) <br /> Diesel 2 19 2 19 0 05 2030 0 15 <br /> Motor Oil ND NO 0 2 200 0 <br /> n Pentacosane (surr) 111 113 1 79 65 125 <br /> SAMPLE SURROGATES <br /> SAMPLE TYPE Sample Client LAB ID 9712009 01E INSTR RUN GC C1971205000000/29/ <br /> INSTRUMENT HP 5890 PREPARED 12/05/97 BATCH ID DSEW120597 2 <br /> UNITS mg/L ANALYZED 12/09/97 DILUTION 1 000000 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> n-Pentacosane (surr) 118 100 118 65 125 <br /> . SAMPLE TYPE Sample Client LAB ID 9712009 02E INSTR RUN GC C1971205000000/30/ <br /> INSTRUMENT HP 5890 PREPARED 12/05/97 BATCH ID DSD120597 2 <br /> UNITS mg/L ANALYZED 12/09/97 DILUTION 1 000000 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> n Pentacosane (surr) 1i1 100 111 65 125 <br />