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May 14, 2012 Lab ID : STK1233666 <br /> Musco Family Olive Environmental Customer : 3-11544 <br /> Quality Control- Inorganic <br /> Constituent Method Date/ID Type Units Cone. QC Data DQO Note <br /> et Chem <br /> Sulfate 300.0 05/01/12:204725CHL MSRPD mg/L 100.0 0.3% <12.3 <br /> 300.0 05/01/12:206239CHL CCB ppm -0.54 2 <br /> CCV ppm 50.00 104% 90-110 <br /> CCB ppm -0.58 2 <br /> CCV PPM 50.00 105% 90-110 <br /> monis Nitrogen 4500NH3B 05/07/12:204921CJJ Blank mgt ND <02 <br /> LCS mg/L 6.000 84.2% 63-116 <br /> MS mg/L 6.000 95.4% 17-127 <br /> (CH 1272321-001) MSD mg/L 6.000 98.8% 17-127 <br /> MSRPD m 6.000 3.6°/ 580.2 <br /> 4500NI1313 101101/12:206561AMB CCB mg/L 0.060 0.2 <br /> CCV mg/L 2.000 109% 90-110 <br /> CCB mg/L 0.058 0.2 <br /> CCV m 2.000 109% 90-110 <br /> itrite as Nitrogen 450ONO2B MS mgt 0.2284 96.3% 1-173 <br /> (CH 1272258-001) MSD mgt 0.2284 94.5% 1-173 <br /> MSRPD mgJL 0.2284 0.0041 <_0.1 <br /> 450ONO2B 04/28/12:206358SBL CCV mg/L 0.1522 102% 90-110 <br /> CCB mg/L 0.001 0.1 <br /> CCV mg/L 0.1522 101% 90-110 <br /> CCB m9JL 0.003 0.1 <br /> Nitrate+Nitrite as 450ONO3F MS mgfL 4.000 92.2% 5-285 <br /> (CC 1281325-001) MSD mgfL 4.000 94.2% 5-285 <br /> MSRPD mg/L 4.000 1.4% <_30.4 <br /> MS mg/1. 4.000 99.3% 5-285 <br /> (STK1233666-002) MSD mg/L 4.000 99.7% 5-285 <br /> MSRPD m 4.000 0.3% 530.4 <br /> 450ONO3F 03/08112:206573AMB CCB mg/L 0.040 0.1 <br /> CCV mg/L 4.000 103% 90-110 <br /> CCB mg/L -0.027 0.1 <br /> CCV mg/L 4.000 105% 90-110 <br /> BOD 52108 04/27/12:300251 SA RgBlk mg/L 0.68 2b <br /> RgBlk mg/L 0.71 2 b <br /> LCS mg/L 198.0 108% 84.6-115 <br /> LCS mgt 198.0 109% 84.6-115 <br /> (STKI233635-001) Dup mg/L 4.3% 15.9 <br /> (STK1233635-001) Du m Il.l% 15.9 <br /> 5210B OS/02/12:300255CTH CCV m L 1.000 99.0% 80-120 <br /> Definition <br /> ICB :Initial Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> CCB :Continuing Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. <br /> RgBlk :Method Reagent Blank-Prepared to correct for any reagent contributions to sample result. <br /> LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery. <br /> MS :Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample <br /> matrix affects analyte recovery. <br /> MSD :Matrix Spike Duplicate of MS/MSD pair-A random sample duplicate is spiked with a known amount of analyted.The recoveries <br /> are an indication of how that sample matrix affects analyte recovery. <br /> Dup :Duplicate Sample-A random sample with each batch is prepared and analyzed in duplicate.The relative percent difference is an <br /> indication of precision for the preparation and analysis. <br /> MSRPD :MS/MSD Relative Percent Difference(RPD)-The MS relative percent difference is an indication of precision for the preparation <br /> and analysis. <br /> ND :Non-detect-Result was below the D O listed for the anal e. <br /> Page 10 of I1 <br />