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j <br /> i <br /> i <br /> North Coast Laboratories, Ltd. Date: 27-Nov-2007 <br /> CLIENT: J.L.Analytical Services <br /> Work order: 0711202 C SUMMARY RE j <br /> Project: 11-509 Laboratory Control Spike <br /> I <br /> Sample ID: LCS-19245 Batch ID: 19245 Test Code: BTXES Units: pg/g Analysis Date 11!16!,071:02:05 PM Prep Date: 11/12/07 <br /> Client ID: Run ID- ORGC8_071116A SegNo: 723487 <br /> i <br /> Analyte Result Limit SPK value SPK Ref Vat %Rea Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] <br /> MTBE 0.4037 0.050 0.400 0 101% 71 126 0 i <br /> Benzene 0.05366 0.0050 0.0500 0 107% 74 126 0 <br /> Toluene 0.05706 0.0050 0.0500 0 114% 82 134 0 <br /> Ethylbenzene 0.05151 0.0050 0.0500 0 103% 82 122 0 <br /> m1p Xylene 0.1010 0.0050 0.100 0 101% 80 132 0 <br /> o-Xylene 0.05048 0.0050 0.0500 0 101% 81 116 0 <br /> Cis-1,2-Dichloroethylene 0.924 0.10 1.00 0 92.4% 73 120 0 i <br /> Sample I1�- LCSD-19245 Batch ID:19245 Test Code: BTXES Units: pglg Analysis Date 11/16/071:36:40 PM Prep Date: 11/12/07 <br /> Client ID: Run ID: ORGC8_07111'6A SegNo: 723488 <br /> Analyte Result Limit SPK value SPK Ref Val %Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> MTBE 0.4052 0.050 0.400 0 101% 71 126 0.404 0.378% 15 <br /> Benzene 0.05318 0.0050 0.0500 0 106% 74 126 0.0537 0.897% 15 <br /> Toluene 0.05622 0.0050 0.0500 0 112% 82 134 0.0571 1.48% 15 <br /> Ethylbenzene 0.05121 0.0050 0.0500 0 102% 82 122 0.0515 0.593% <br /> 15 <br /> m,p-Xylene 0.1003 0.0050 0.100 0 100% 80 132 0.101 0.694% 15 <br /> oaXylene 0.05096 0.0050 0.0500 0 102% 81 116 0.0505 0.946% 15 <br /> i Cis-1,2-Dichloroethylene 0.934 0.10 1.00 0 93.4% 73 120 0.924 1.10% 15 <br /> Sample ID: LCS-19239 Batch ID: 19239 Test Code: TPHDIS Units: pg/g Analysis Date 11/19107 1:30:05 AM Prep Date: 11/12107 <br /> ` Client ID: Run ID: ORGC14_071119A SegNo: 724430 <br /> I Analyte Result Limit SPK value SPK Ref Val %Rec LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> j TPHC Diesel(C12-C22) 11.48 1.0 10.0 0 115% 67 122 0 <br /> N-Tricosane 1.22 0.10 1.00 0 122% 56 130 0 <br /> I <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank <br /> I <br /> J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits <br /> I <br />