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6) <br /> W <br /> 23-Aug-2007 <br /> g-2007 <br /> North Coast Laboratories,Ltd. DaLn <br /> IQ <br /> M <br /> CLIENT: J L Analytical Services QC SUMMARY REPORT CS) <br /> J <br /> Work Order; 0708352 Laboratory Control Spike (S) <br /> Project: B-858 <br /> w <br /> Sample 10: 4CS-iB723 Bitch to:18123 Test Code- STXES Units: Pg1g Analysis Date 8021!2007 6:36:29 PM Prop Date-b12112011 <br /> Client 10: Run ID: 0R()C81r7082I13 SeqNo: 702106 <br /> Analyte Result Limit SPK value SPK def Val %Rec Lowl-imit Highl-innR RPD ReF Val %RPD RPOLinnit Qua] LO <br /> LTI <br /> w <br /> MTBE 0.4611 0.050 0.400 0 115% 79 0 S M <br /> w <br /> Berizene 4-05732 0`0050 0.0100 0 1115% 82 117 0 U) <br /> Toluene 6.06,195 0.0050 0.0900 0 124% 84 129 <br /> Ethylbenzene 0.05792 0.0050 0.0600 0 116% 86 119 0 <br /> m.p-Xylene 0.1198 0M50 0.100 0 120% 83 Ili 0 S. <br /> o-Xylene 0.05445 0.0050 0.0500 0 1090/0 83 119 a <br /> Cis-1,2-Dichlorce[hylene 0.897 0.10 1.00 0 89-7% 79 125 0 <br /> Sample ID: LCSD-1 9723 Batch ID: 18723 Test Code: BTXES Units' pglg Analysis Date MUM?7:12,10 PM Prep CaW 812112007 <br /> Client 10: Run ID: ORGCO0709218 SeqNo: 70201 <br /> Analyte Result limit SPK value SPK Rel Val %Ree LoMJmit Highl-imit RPI)Ref Val %RPO RP OlLimit atral <br /> MTBE 0.4539 0.050 OADO 0 113% 79 112 0-461 1.57% 15 S <br /> Benzene 0.05704 0.0050 0-0500 0 114% 82 117 0.0573 0.487% 15 <br /> Toluene 0.0083 0.0050 0.0500 0 122% 84 129 0.0620 1.82% 15 <br /> Ethylbenzene 0.05723 0-0050 0.0900 0 114% 86 119 0.0579 1.20% 15 <br /> m.p-Xylene 0.1176 0.0050 0,100 0 118% 83 111 0.120 1.90% 15 S <br /> o-Xylene 0.05378 0.0050 0.0500 0 108% 83 119 0-05" 1.23% 15 <br /> Cis-1,2-Dichtoroethylene 0.905 0.10 1.00 0 90.5% 79 125 0.897 0.932% is <br /> Sample ID: LCS-13723-G Batch tD: 18723 Test Code: TPHCGS Units: Ugig Analysis Date 812112007 7:47:43 PM Prep Date: 812112007 <br /> Client 10: Run ID: OROCS-070821A SeqNc: 792927 <br /> Analyte Result Limit SPK value SPK Ref Val %Ree Lowl-imit HighLimit RPD Ref Val %RPD RPDLimR Oual <br /> TPHC Gas(G6-C14) 9.816 1.0 10.0 0 98.2% 92 129 0 <br /> T <br /> 1> <br /> Qualillem. ND-Not Detected at the.Reporting Lank S-Spike Rewveiy outside accepted remery limits B-Analyte detected is the associated Nicthad Blank C)M <br /> J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits <br /> 01 <br />