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North Coast Laboratories, Ltd. Date: 23-Aug-2007 <br /> CLIENT: J L Analytical Services QC SUMMARY REPORT <br /> Work Order: 0708352 <br /> Project: 8-858 Method Blank <br /> Sample ID: MB-18723 Batch ID: 18723 Test Code: BTXES Units: pg/g Analysis Date 8/21/2007 9:33:39 PM Prep Date: 8/21/2007 <br /> Client ID: Run ID: ORGC8_070821B SegNo: 702957 <br /> Analyte Result Limit SPK value SPK Ref Val %Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> MTBE ----- --- ND 0.050 ------- ---- - ------- — <br /> Benzene ND 0.0050 <br /> Toluene ND 0.0050 <br /> Ethylbenzene ND 0.0050 <br /> m,p-Xylene ND 0.0050 <br /> o-Xylene ND 0.0050 <br /> Cis-1,2-Dichloroethylene 0.848 0.10 1.00 0 84.8% 79 125 0 <br /> Sample ID: MB-18723 Batch ID: 18723 Test Code: TPHCGS Units. pg/g Analysis Date 8/21/2007 9:33:39 PM Prep Date: 8/21/2007 <br /> Client ID: Run ID: ORGC8_070821A SegNo: 702929 <br /> Analyte Result Limit SPK value SPK Ref Val %Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> TPHC Gas(C6-C14) ND 1.0 <br /> Sample ID: MB-18682 Batch ID: 18682 Test Code: TPHDIS Units: pg/g Analysis Date 8/19/2007 3:01:04 AM Prep Date: 8/16/2007 <br /> Client ID: Run ID: ORGC14_070819B SegNo: 702014 <br /> Analyte Result Limit SPK value SPK Ref Val %Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] <br /> TPHC Diesel(C12-C22)---- -- ND ----1.0 -- - -- - - <br /> N-Tricosane 0.938 0.10 1.00 0 93.8% 70 120 0 <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank <br /> J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits <br />