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1& 0 0 <br /> AFF M6 J L ANALYTICAL SERVICES, <br /> . <br /> ul 217 Primo Way • P.O.Box 576185 • Modesto,California 95357 <br /> Office(209)538-8111 . FAX(209)538-3966 <br /> 27 July 1995 <br /> POSDEF Power Co, LP <br /> ATTN: Ed Stockton <br /> 2526 W. Washington St. <br /> Stockton CA 95203 <br /> Dear Sir, <br /> The following is a report on the activities performed by a representative of <br /> JL Analytical Services, Inc. over a period of 9 days starting with 17 July 1995, in <br /> relation to the Sulfuric Acid spill. <br /> The morning of Monday 17 July 1995, Mark Jacobs of JL Analytical was contacted by <br /> Ed Stockton of P.O.S.D.E.F. Mr. Stockton indicated there had been a spill of Sulfuric <br /> Acid onto an area of soil. He indicated that Ericson Environmental was already on site <br /> and had begun removing soil presumed to be contaminated. Ed explained the role of <br /> JL Analytical would he to determine the extent of the contamination and to direct the <br /> efforts of Ericson personnel to ensure they removed the contaminated soil. <br /> Upon arrival to the site, Mr. Jacobs was provided with appropriate safety gear and <br /> resources with which to perform the testing for pH. An Orion model SA 250 pH meter <br /> with an Innovative Sensors, Inc., SOTA pH electrode was utilized to perform the <br /> analyses. The meter was calibrated by standard procedures. <br /> The first step was to determine the background pH level of the soil. The soil was <br /> sampled at a depth of one foot below the surface at the cooling towers, the air dryers, <br /> and by the auxiliary steam generator. The pH values at those sites were 7.2, 6.8, and <br /> 7.3 respectively. See attachment number eight for the site map. <br /> The next step was to sample the soil in the area of the Sulfuric Acid tank to determine <br /> where more soil should he removed. The soil was sampled at seven locations. Please <br /> reference attachment number one. The data for the sites is referenced on attachment <br />