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CS <br /> North Coast Laboratories,Ltd. Date: 23-Aug-2007 <br /> U <br /> CLIENT: J L A.nalytiW Services CSU P � a <br /> Work Order: 0708353 <br /> Project: 8.839 Laboratory Control Spike Q <br /> fi <br /> Sample 10: LCS-98723 9iitch ID: 18323 Test Cade: BTKES Units: ygtg Analysis Date 812112007 6:36:29 PM Prep flats: 12112007 <br /> Client to: Run 10: 0RGC8rd7082iB SegNo: 702416 <br /> Analyte Result Limit SPK value SPK F(ef Val %Rec LotivLimit Kight.imit RPO Ref Val '¢.RPD RPDLimA Dual ,®o <br /> U1 <br /> WOE 0.4611 0.050 0.400 0 1 t5% 79 •112 0 S m <br /> W <br /> Benzene 6.05732 0:0050 0A00 0 1'15% 82 117 0 <br /> Toluene d.00195 0.0050 0.0600 0 124% 84 129 0 <br /> Ethylbenzere 6.05792 0.0050 0.0900 0 1166 86 119 0 <br /> m,p-Xylene 0.1198 0.0050 0.100 0 1200% 83 111 0 S <br /> a•Xylene 0.05445 0.0050 0.0500 0 109% 83 119 0 <br /> Cis-1,2-Dichloraethylene 0.891 0.10 1.00 0 89.7;6 79 125 0 <br /> Sample 10: LCSD-18723 Batch LD: 18723 Test Code' BTXES Units: PS19 Analysis Date 8/21)2007 7.12.10 PM Prep Date: 812112007 <br /> Client 10: Run ID: ORGC8 0708218 SegNo: 702951 <br /> Analyte Result .w Limit SPK value SPK Ref Val %Rec LotivLimit Highl-imit RPD Ref Val %RPD RPDLinnil Oval <br /> r <br /> MTBE 0.4539 0.050 0.400 0 113% 79 112 0.461 1.57% 15 S D <br /> Benzene 0.05704 0.0050 0.0500 0 114% 82 117 0.0573 0.487% 15 <br /> Toluene 0.06083 0.0050 0.0500 0 122% 84 129 0.0620 1.82?A 15 { <br /> Elhylbenzene 0.05723 0.0050 0.0500 0 114% 86 119 0.0579 1.20% 15 H <br /> m,p-Xylene 0.1176 0-0050 0.100 0 119% 83 111 0.120 1.90% 15 S D <br /> P- <br /> o-Xylene 0.05378 0.0050 0.0500 0 105% 83 119 0.0544 1.23% 15 <br /> Cis-1,2-Dichlomethylene 0.905 0.10 1.00 0 9D.5% 79 125 0.897 0.932°,x® 15 <br /> Sample 10: LC348723-G Batch IU:18723 Test Code: TPHCGS Units: pgig Analysis Dale 812112007 7.47-43 PM Prep Date:812112007 <br /> Client to: Run ID: ORGC8_070821A SegNo: 702927 <br /> Analyte Result Limit SPK value SPK Ref Val %Rec Lo A imit Hight-imit RPD Ref Val %RPD RPOUmit Dual <br /> TPHC Gas{C(i-C14) 9.816 1.0 10.0 0 98.2°% 92 129 0 <br /> D <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits 8-Analyte detected in the associated Method Blank m <br /> 1-Analyte detected below quantitation limits R.RPD outside accepted recovery limits N <br /> b <br /> r <br /> m <br /> �.n <br />