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CLIENT: J L Analytical Services — <br /> Work Order: 0708352 QC SUMMARY REPORT <br /> Project: 8-858 Laboratory Control Spike Duplicate <br /> Sample ID: LCSD-18723-G Batch ID: 18723 Test Code: TPHCGS Units: pg/g Analysis Date 8/2112007 8:23:09 PM Prep Date: 8/21/2007 <br /> Client ID: Run ID: ORGC8_070821A SegNo: 702928 <br /> Analyte — — Result Limit SPK value SPK Ref Val %Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> TPHC Gas(C6-C14) 9.547 --- 1.0 10.0 0 95.5% 92 129 9.82 2.79% 15 — <br /> Sample ID: LCS-18682 Batch ID: 18682 Test Code: TPHDIS Units: pg/g Analysis Date 8/19/2007 1:07:52 AM Prep Date: 8/1612007 <br /> Client ID: Run ID: ORGC14_0708198 SegNo: 702010 <br /> Analyte -- --- -- Result Limit SPK value SPK Ref Val %Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> TPHC Diesel(C12-C22) 8.559 1.0 10.0 0 85.6% 70 120 0 <br /> N-Tricosane 0.944 0.10 1.00 0 94.4% 70 120 0 <br /> Sample ID: LCSD-18682 Batch ID: 18682 Test Code: TPHDIS Units: pg/9 Analysis Date 8119/2007 1:26:46 AM Prep Date: 8/16/2007 <br /> Client ID: Run ID: ORGC14_070819B SegNo: 702011 <br /> Analyte --- -- — Result Limit SPK value SPK Ref Val % Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> TPHC Diesel(C12-C22) 8.696 1.0 10.0 0 87.0% 70 120 8.56 1.58% 15 <br /> N-Tricosane 0.924 0.10 1.00 0 92.4% 70 120 0.944 2.17% <br /> 15 <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank <br /> J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits <br />