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North Coast Laboratories, Ltd. Date: 23-Aug-2007 <br /> CLIENT: J L Analytical Services - ---- - __ <br /> Work Order: 0708353 QC SUMMARY REPORT <br /> Project: 8-859 Laboratory Control Spike <br /> Sample ID: LCS-18723 Batch ID: 18723 Test Code: BTXES Units: pg/g Analysis Date 8/21/2007 6:36:29 PM Prep Date: 8/2112007 <br /> Client ID: Run ID: ORGC8 0708218 <br /> - SegNo: 702936 <br /> Analyte - - Result Limit SPK value SPK Ref Val %Rec LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> MTBE 0.4611 --0.050 0.400 0 115% 79 112 0 --- -- - <br /> Benzene S <br /> 0.05732 0.0050 0.0500 0 <br /> 115% 82 117 0 <br /> Toluene 0.06195 0.0050 0.0500 0 124% 84 129 <br /> Ethylbenzene 0 <br /> 0.05792 0.0050 0.0500 0 116% 86 119 0 <br /> o-Xylene <br /> lene 0.1198 0.0050 0.100 0 120% 83 111 p <br /> o-Xylene g <br /> 0.05445 0.0050 0.0500 0 109% 83 119 0 <br /> Cis-1,2-D ichloroethylene 0.897 0.10 1.00 0 89.7% 79 125 <br /> 0 <br /> Sample ID: LCSD-18723 Batch ID: 18723 Test Code: BTXES Units: pg/g Analysis Date 8/21/2007 7:12:10 PM Prep Date,; 8/21/2007 <br /> Client ID: Run ID: ORGC8 0708218 <br /> - SegNo: 702951 <br /> Analyte Result Limit SPK value SPK Ref Val % Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> MTBE 0.4539 0.050 0.400 0 113% 79 1120461 --- <br /> Benzene 0.05704 0.0050 0.0500 0 114/°° 82 117 15 S <br /> . 1.57% <br /> Toluene 0.0573 0.487% 150.06083 0.0050 0.0500 0 122% 84 129 0.0620 1.82% <br /> Ethylbenzene 15 <br /> 0.05723 0.0050 0.0500 0 114% 86 119 0.0579 1.20% 15 <br /> o-Xylene <br /> leve 0.1176 0.0050 0.100 0 118% 83 111 0.120 1.90% 15 S <br /> o-Xylene 0.05378 0.0050 0.0500 ° <br /> 0 108% 83 119 0.0544 1.23% 15 <br /> Cis-1,2-Dichloroethylene 0.905 0.10 100 ° <br /> 0 90.5% 79 125 0.897 0.932% 15 <br /> Sample ID: LCS-18723-G Batch ID: 18723 Test Code: TPHCGS Units. pg/g Analysis Date 8/21/2007 7:47:43 PM Prep Date: 8/21/2007 <br /> Client ID: Run ID: ORGC8 070821A <br /> - SegNo: 702927 <br /> Analyte - -- Result Limit SPK value SPK Ref Val %Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> TPHC Gas(C6-C14) 9.816 -- - 1.0 10.0 0 ° - -- -------- -- <br /> 98.2/° 92 129 0 <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank <br /> 1-Analyte detected below quantitation limits R-RPD outside accepted recovery limits <br />