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SAO �N ACCC9�4ry <br />4 <br />Y <br />ANALYTICAL 1LY 1 IC[ 1L Cl iEl lIS 1 S <br />July 31, 2007 Lab ID STK734832 <br />Customer 3009812 <br />Panella Trucking <br />P.O. Box 5010 <br />Stockton, CA 95205 <br />Laboratory Report <br />Introduction: This report package contains total of 31 pages divided into three sections: <br />Case Narrative <br />(3 <br />Pages) : <br />An overview of the work performed at FGL. <br />Chemical Results <br />(7 <br />Pages) : <br />Results for each sample submitted. <br />Quality Control <br />(21 <br />Pages) : <br />Supporting Quality Control (QC) results. <br />This report package pertains to the following samples: <br />Sampling and Receipt Information: The sampling was performed by FGL using the following <br />methods (where applicable): <br />Bacteriological Sampling - SOFS005 <br />Grab sampling for liquids - SOFS010 <br />Composite sampling for liquids - SOFS015 <br />Grab sampling for solids - SOFS020 <br />Composite sampling for solids - SOFS025 <br />All samples were received, prepared and analyzed within the method specified holding times. <br />All samples were received on ice. All samples were checked for pH if acid or base <br />preservation required (except for VOAs). For details of sample receipt information, please see <br />the attached Chain of Custody and Condition Upon Receipt Forms. <br />Discussion of Analytical Results: <br />NOTE: In regards to test EPA 8270 for sample Steam Cleaner Solids (FGL ID STK <br />734832-02), the benzoic acid result was above calibration. A result within calibration range <br />was analyzed past Hold Time; and it confirmed the original reported result. <br />Quality Control: All samples were prepared and analyzed according to the following tables: <br />Inorganic - Metals QC <br />3050B 06/05/2007:A209 All preparation quality controls are within established criteria, except: <br />The following note applies to Chromium, Molybdenum, Antimony: <br />430 Post Digestion Spike (PDS) not within Acceptance Range (AR) because of matrix <br />interferences affecting this analyte. <br />The following note applies to Molybdenum, Nickel, Antimony: <br />Corporate Offices & Laboratory <br />Date <br />Date FGL Lab <br />Sample Description <br />Sampled <br />Received Sample ID # Matrix <br />Sand Blast Sand <br />06/01/2007 <br />06/01/2007 STK734832-01 Sld <br />Steam Cleaner Solids <br />06/01/2007 <br />06/01/2007 1 STK734832-02 Sld <br />Sampling and Receipt Information: The sampling was performed by FGL using the following <br />methods (where applicable): <br />Bacteriological Sampling - SOFS005 <br />Grab sampling for liquids - SOFS010 <br />Composite sampling for liquids - SOFS015 <br />Grab sampling for solids - SOFS020 <br />Composite sampling for solids - SOFS025 <br />All samples were received, prepared and analyzed within the method specified holding times. <br />All samples were received on ice. All samples were checked for pH if acid or base <br />preservation required (except for VOAs). For details of sample receipt information, please see <br />the attached Chain of Custody and Condition Upon Receipt Forms. <br />Discussion of Analytical Results: <br />NOTE: In regards to test EPA 8270 for sample Steam Cleaner Solids (FGL ID STK <br />734832-02), the benzoic acid result was above calibration. A result within calibration range <br />was analyzed past Hold Time; and it confirmed the original reported result. <br />Quality Control: All samples were prepared and analyzed according to the following tables: <br />Inorganic - Metals QC <br />3050B 06/05/2007:A209 All preparation quality controls are within established criteria, except: <br />The following note applies to Chromium, Molybdenum, Antimony: <br />430 Post Digestion Spike (PDS) not within Acceptance Range (AR) because of matrix <br />interferences affecting this analyte. <br />The following note applies to Molybdenum, Nickel, Antimony: <br />Corporate Offices & Laboratory <br />Office & Laboratory <br />Office & Laboratory <br />Field Office <br />P.O. Box 272 / 853 Corporation Street <br />2500 Stagecoach Road <br />563 East Undo Avenue <br />Visalia, California <br />Santa Paula, CA 93061-0272 <br />Stockton, CA 95215 <br />Chico, CA 95926 <br />TEL: (559) 734-9473 <br />TEL: (805) 392-2000 <br />TEL: (209) 942-0182 <br />TEL: (530) 343-5818 <br />FAX: (559) 734-8435 <br />FAX: (805) 525-4172 <br />FAX: (209) 942-0423 <br />FAX: (530) 343-3807 <br />Mobile: (559) 737-2399 <br />CA NELAP Certification No. 0111 OCA <br />CA ELAP Certification No. 1563 <br />CA ELAP Certification No. 1573 <br />