Laserfiche WebLink
CCailllpbell A11a1VtilCal, IQ(°. 1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />1. R/ 1 Y` 1 Web: www.mccampbell.com E-mail: main@rnccaznpbell.com <br />"When Oualitv Counts" Telephone: 877-252-9262 Fax: 925-252-9269 <br />W.O. Sample Matrix: Solid QC Matrix: Soil WorkOrder: 0807081 <br />EPA Method 6020A <br />Extraction SW3050B <br />BatchlD: 36616 <br />Spiked Sample ID 0807087-001A <br />Analyte <br />Sample <br />mg/Kg <br />Spiked <br />mg/Kg <br />MS <br />% Rec. <br />MSD <br />% Rec. <br />MS -MSD <br />% RPD <br />Spiked <br />mg/Kg <br />LCS <br />% Rec. <br />LCSD <br />% Rec. <br />LCS-LCSD <br />% RPD <br />Acceptance Criteria (%) <br />MS / MSD RPD LCS/LCSD <br />RPD <br />Antimony <br />ND <br />50 <br />96.3 <br />99.3 <br />2.97 <br />10 <br />99.9 <br />99.3 <br />0.592 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Arsenic <br />4.7 <br />50 <br />92.8 <br />96.7 <br />3.78 <br />10 <br />1 97 <br />96.5 <br />0.527 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Barium <br />280 <br />500 <br />91.4 <br />96.4 <br />3.39 <br />100 <br />96 <br />94.7 <br />1.37 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Beryllium <br />0.61 <br />50 <br />80.7 <br />82.5 <br />2.22 <br />10 <br />95.7 <br />94.7 <br />1.04 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Cadmium <br />ND <br />50 <br />92.4 <br />95.3 <br />3.13 <br />10 <br />98.5 <br />97.9 <br />0.631 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Chromium <br />44 <br />50 <br />83.6 <br />89.7 <br />3.45 <br />1 10 <br />101 <br />99.8 <br />1.25 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Cobalt <br />14 <br />50 <br />90 <br />93.6 <br />3.01 <br />10 <br />95.4 <br />95.7 <br />0.272 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Copper <br />Lead <br />26 <br />5.7 <br />50 <br />50 <br />88.3 <br />88.5 <br />92.6 <br />91.9 <br />2.99 <br />3.39 <br />10 <br />10 <br />98.5 <br />94.5 <br />98.1 <br />93.9 <br />0.417 <br />0.669 <br />70- 130 <br />70-130 <br />20 <br />20 <br />80- 120 <br />80-120 <br />20 <br />20 <br />Mercury <br />ND <br />1.25 <br />88 <br />91.1 <br />3.42 <br />0.25 <br />92 <br />91.4 <br />0.611 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Molybdenum <br />2.1 <br />50 <br />92.8 <br />97.1 <br />4.40 <br />10 <br />97.3 <br />95.6 <br />1.72 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Nickel <br />37 <br />50 <br />88.6 <br />93.2 <br />2.79 <br />10 <br />97.4 <br />1 96.1 <br />1.33 <br />70- 130 1 <br />20 <br />80- 120 <br />20 <br />Selenium <br />Silver <br />ND <br />ND <br />50 <br />50 <br />89.3 <br />102 <br />92.9 <br />106 <br />3.99 <br />3.32 <br />10 <br />10 <br />96.1 <br />98.7 <br />97.1 <br />98.3 <br />0.963 <br />0.376 <br />70- 130 <br />70- 130 <br />20 <br />20 <br />80- 120 <br />80- 120 1 <br />20 <br />20 <br />Thallium <br />ND <br />50 <br />93.3 <br />95.6 <br />2.44 <br />10 <br />88.6 <br />88.4 <br />0.249 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Vanadium <br />120 <br />50 <br />68.2, F1 <br />76.4 <br />2.69 <br />10 <br />100 <br />99.4 <br />0.832 1 <br />70- 130 <br />20 <br />80- 120 <br />20 <br />Zinc 66 500 94.2 97.6 3.17 100 96.6 96.5 0.104 1 70- 130 20 <br />%SS: 105 250 96 98 1.93 250 99 97 1.91 70- 130 20 <br />All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br />NONE <br />80- 120 <br />1 70- 130 <br />20 <br />20 <br />171 = MS / MSD outside of acceptance criteria. LCS - LCSD validate prep batch. <br />BATCH 36616 SUMMARY <br />Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br />0807081-OOIA 06/30/08 07/02/08 07/03/08 8:51 PM I 0807081-OOIA 06/30/08 07/02/08 07/03/08 8:59 PM <br />MS = Matrix Spike; MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Same Duplicate; RPD = Relative Percent Deviation. <br />% Recovery = 100 ` (MS -Sam) / (Amount Spiked); RPD = 100' (MS - MSD) / ((MS + MSD) / 2). <br />MS / MSD spike recoveries and / or %RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample is inhomogenous <br />AND contains significant concentrations of analyte relative to the amount spiked, or b) the spiked sample's matrix interferes with the spike recovery. <br />N/A = not applicable to this method. <br />NR = analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte <br />content. <br />