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DEMENNO/KERDOON <br /> P.E 4300 ICP <br /> QA REPORT FORM <br /> DATE: 11/7/2014 ANALYST: JL <br /> ANALYTE ICV %REC. ICB ICSA/SIC1 %REC. ICSAB/SIC2 %REC LCS THEORI LCS ACTUAL %R CCV-1 %REC <br /> Pb 974 97.4 <25.0 514 102.8 458 91.6 100 102.0 102.0 941 94.1 <br /> Cu 1010 101.0 <25.0 507 101.4 465 93.0 100 99.7 99.7 989 98.9 <br /> Zn 992 99.2 <25.0 529 105.8 491 98.2 100 105.0 105.0 978 97.8 <br /> TI 989 98.9 <25.0 510 1 102.0 477 95.4 100 98.2 98.2 952 95.2 <br /> As 968 96.8 <25.0 521 104.2 465 93.0 100 98.4 98.4 931 93.1 <br /> Cr 982 98.2 <25.0 517 103.4 478 95.6 100 98.8 98.8 957 95.7 <br /> Ni 986 98.6 <25.0 509 101.8 458 91.6 100 98.4 98.4 969 96.9 <br /> Cd 1 990 99.0 <25.0 518 103.6 1 492 98.4 100 99.6 99.6 978 97.8 <br /> Ag 1001 100.1 <25.0 508 101.6 469 93.8 100 99.4 99.4 984 98.4 <br /> Ba 986 98.6 <25.0 513 102.6 472 94.4 100 100.0 100.0 961 96.1 <br /> Se 976 97.6 <25.0 517 103.4 456 91.2 100 100.0 100.0 941 94.1 <br /> Be 992 99.2 <25.0 527 105.4 492 98.4 100 99.0 99.0 964 96.4 <br /> Mo 968 96.8 <25.0 504 100.8 488 97.6 100 97.3 97.3 944 94.4 <br /> Sb 981 98.1 <25.0 501 100.2 471 94.2 100 95.1 95.1 945 94.5 <br /> V 978 97.8 <25.0 508 101.6 502 100.4 100 98.9 98.9 953 95.3 <br /> Co 979 1 97.9 <25.0 1 523 104.6 475 1 95.0 100 98.4 98.4 956 1 95.6 <br /> Sn 958 1 95.8 <25,0 494 98.8 453 90.6 100 95.8 95.8 927 92.7 <br /> i ICV.-INITIAL CALIBRATION VERIFICATION ICSA=INTERFERENCE CHECK STD A <br /> 7 <br /> CCV.-CONTINUING CALIBRATION VERIFICATION ICSAB=INTERFERENCE CHECK STD B <br /> ICB.-INITIAL CALIBRATION BLANK %R CRITERIA ON SIC1 85-115% <br /> CCB.-CONTINUING CALIBRATION BLANK %R CRITERIA ON SIC2 85-115% <br /> %CRITERIA ON ICV 95-105% LCS=LABORATORY CONTROL SAMPLE <br /> %CRITERIA ON CCV85-115% RESULTS IN PPB v <br /> MDL.-METHOD DETECTION LIMIT f-' <br /> CHECKED BY: DATE: <br /> REVIEWED BY: DATE: �� <br />