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01/05/2005 12:35 2095720916 GEO PAGE 15/23 <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Pax(209)572-0916 <br /> Report# Q352-02 CERTIFICATE OF ANALYSIS Date: 12/21/04 <br /> Thorpe Oil Date Res'd: 12/17/04 <br /> Date Started. 21/04 <br /> PO Box 357 Proje&. 111919 Lower Sacramento Rd,Lodi Ca Date Completed:12/21/04 <br /> Lodi CA 95241 <br /> Date Sampled: 12/17/04 <br /> PO# Time: 10.30 am <br /> Sample ID: SP-West Sampler: R.Ciuun(Geo) <br /> Lab ID: Q201845 <br /> Method_ RL Analyte Results units <br /> 8260B 5.0 Benzene ND µ8 <br /> 5.0 Toluene ND <br /> 5.0 Ethyl Benzene ND <br /> 5.0 Total Xylenes ND <br /> 10 Methyl tert-butyl ether(MOE) ND <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl teat-butyl ether(ETRE) ND <br /> 10 tent-Amyl methyl ether(TAW ND <br /> Surrogate Anud Spiked Anant Rer- %Recovery Cc Limit% <br /> 1,2-Dichloroethane-d4 20 21.5 107.5 66-133 <br /> 2-Bromo-l-chloropropane 20 22.0 110.0 63-139 <br /> 4-Bromofluorobenzen.e 20 17.7 88.5 64.136 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification #2585 Laboratory Director <br />