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i
<br />0IMUM VERIFICATION LABORATO AL V]:JVII II
<br />All inalyses methods are designated EPA methods described In EPA SW 846, Third Edition. Those methods not found in
<br />SW ,4=16, are specifically noted below. Refer to the "SWRCB LUFT Field Manual% Appendix A-20, Table 3-5 for detection
<br />limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for Initini
<br />Evaluation and Investigation of UST's" for the waste and motor oil detection limits.
<br />Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted.
<br />l"$'ever inboratory shall utilize the most conservative method.
<br />LA130RATORY ANALYSES TERMINOLOGY:
<br />TP11-(;
<br />TPI1-1)Total
<br />Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260
<br />13'1',X &, E
<br />Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260
<br />Benzene, Toluene, Xylene & Ethyl Benzene, GC/PID
<br />CL I K'
<br />8020 or GC/MS 8260
<br />Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240
<br />v—
<br />4j
<br />FDR
<br />Gr' FII)
<br />TANK
<br />TANK
<br />TPH-G
<br />TPH-D
<br />BTX d't E
<br />CL HC
<br />TOTAL
<br />"0
<br />+fR_4LS
<br />PCB
<br />Soxhlet sample preparation
<br />CONTENTS
<br />8015
<br />8015
<br />8020
<br />8010
<br />LEAD
<br />ICAP/
<br />8270
<br />8260
<br />8260
<br />8260
<br />8240
<br />7420 EN
<br />$g22440�
<br />IRONM
<br />Sr
<br />11
<br />8080
<br />7421An
<br />LF..ADED
<br />GAS
<br />X
<br />X
<br />X
<br />X
<br />UNL GAS
<br />X
<br />X
<br />_
<br />DIESEL
<br />X
<br />X
<br />KEROSENE
<br />X
<br />X
<br />_
<br />UNK FUEL
<br />X
<br />X
<br />X
<br />X
<br />OIL
<br />X
<br />X
<br />CHLOR.
<br />SOLVENTS
<br />X
<br />X
<br />'
<br />NONCNLOR
<br />SOLVENTS
<br />X
<br />WASTE\
<br />USED OIL
<br />X
<br />X
<br />X
<br />X
<br />X
<br />All inalyses methods are designated EPA methods described In EPA SW 846, Third Edition. Those methods not found in
<br />SW ,4=16, are specifically noted below. Refer to the "SWRCB LUFT Field Manual% Appendix A-20, Table 3-5 for detection
<br />limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for Initini
<br />Evaluation and Investigation of UST's" for the waste and motor oil detection limits.
<br />Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted.
<br />l"$'ever inboratory shall utilize the most conservative method.
<br />LA130RATORY ANALYSES TERMINOLOGY:
<br />TP11-(;
<br />TPI1-1)Total
<br />Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260
<br />13'1',X &, E
<br />Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260
<br />Benzene, Toluene, Xylene & Ethyl Benzene, GC/PID
<br />CL I K'
<br />8020 or GC/MS 8260
<br />Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240
<br />To'f*,V. L.FAD
<br />Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />FDR
<br />Gr' FII)
<br />Ethviene dibromide (DHS -AB 1803), GC/MS 8240 (DHS -Luft)
<br />WAP ttr AA
<br />Gas Chromatography, Flame Ionization Detection
<br />Inductively Coupled Plasma Atomic Emission Spectrometry
<br />PCil
<br />6010 or Atomic Absorption
<br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lend, Zinc and Nickel.
<br />W111od 3050
<br />Polychlorinated Biphenyls, GC/MS 8270 or 8080
<br />Acid digestion
<br />Nicillod 3510
<br />Soxhlet sample preparation
<br />Method 1550
<br />Sonication sample preparation, extraction method
<br />5030
<br />Purge and trap sample preparation
<br />QA/Q(-
<br />Quality Assurance/Quality Control
<br />r4wes: To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns ire
<br />preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons
<br />h;tee been characterized and proper QA/AC is followed.
<br />For Drinking water sources, FPA recommends that the 500 Series for volatile organics be used In preference to the 600 series
<br />because the detection lintits are lower the QA/QC is better.
<br />r:ii 2, Od8 (Rev 2/8/91)
<br />Page 8
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