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MINI Til VEIRWICATION�LA130RATORY ANALYSIS <br /> OXYGEN <br /> TANK TANK TP -G TPH-D BTX&E CL HC TOTAL MTBE ATES MWAL PCB <br /> # CONTENTS 8015 8015 8020 8010 LEAD 8020 (MTBE, ICAPI 8270 <br /> 8264 8260 $260 $240 7420 8260 E.rsE,TBA,DiPE, AES or 8080 <br /> 8260 7421 rAME) AA <br /> 8260 <br /> GAS X X x X <br /> UNL GAS X X X <br /> DIESEL X X <br /> KEROSENE X X X <br /> UNKFUEL X X X X X <br /> PROD.OIL X X X <br /> CHLOR. X <br /> SOLVENTS X X <br /> NONCHLOR X <br /> SOLVENTS X X <br /> W <br /> LASTE\ <br /> USED OIL X X X X X X X <br /> All analysis methods am the designated.EPA methods described in EPA SW 846,Third Edition. methods not found in SW 846 amre <br /> specifically noted belowRefer to the"S CB LUFT Field Manual",Appendix D(B),Table 3-5 on page A20 for trummum.detection <br /> 'limits for motor vehicle fuel diesel). Refer to "Th-Regional Board Staff Recommendations for 1nittal Evaluation and <br /> investigation of USre for the waste and motor oil nummum detection limits Detection Limits that remain below the MCL,STLC or <br /> Allowable Limit of the contummant is question will be accepted,however laboratery shall uJilize the most eo tine <br /> LABORATORY ANALYSES TERMINOLOGY- <br /> TPH-G Total Petroleum Hydrocarbon,Gasoline, (5030)8015 mod or GUM 8260 <br /> TPH-D Total Petroleum Hydrocarbcw6 Diesel,GCIFID(3550),8015 mod or GUMS 8260 <br /> BTX&E Toluene,Xylene&Ethyl Benzene,GCMID 9=or GUMS 8260 <br /> CL HC ChlodnaftdHydmcwbonGCAFISDSOIO.GCAWSS240or8260 <br /> TOTALLEAD Total lead,AA 7420, AA 7421 or 1CP-AES 6010 <br /> OXYGENATES E,ETHE,TAME.DIPF,&TBA GUMS 8260(For MTBE s==only you may use 8020) <br /> METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Metals: <br /> Cadrufain,Chromium ID and VT,Lead,Zinc and Nickel. <br /> PCB Polychlorinated B' Is,GCftM 8270 or 8080 <br /> GC-FID Gas Chromatography,Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 So et sample preparation <br /> Method 3550 Sonication sample preparation,extraeflon.method <br /> M 5030 Purge and trap smWle preparation <br /> QQuality AmmancelQuality Control <br /> Notes: To avoid false positive detection of benzene,benzenotm solvents are to be used. Fused capilloy columns are preferred to packed columns,a <br /> packed column may be used as a cat"with"dirty" have been characterized and proper QAJQC is followed. For <br /> drinking water sources,EPA recommends that the 500 series for volatile o 'c should be used in preference to the 600 series becituse the detection <br /> limits are lower and the Q is boner. Samples exhibiting any level of heavy metal contsminstion may require further analysis. <br /> recommends holding those samples until disposal is inti <br /> EH 23 046 (R ) <br /> 5 <br />