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MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> OXYGEN <br /> METAL PCB <br /> TANK TANK TPH-G TPH-D BTX&E CL HC TOTAL MTBE ATES <br /> # CONTENTS 8015 8015 / 8270 <br /> 8020 8010 LEAD 8020 TBA DIPE, AES BE Por 8080 <br /> 8260 8260 8260 8240 7420 8260 ETBE, AA <br /> 8260 7421 TAME) <br /> 8260 <br /> LEADED GAS X <br /> X }{ X <br /> X <br /> UNL GAS X X <br /> DIESEL X X <br /> X <br /> KEROSENE X X <br /> UNK FUEL X <br /> X X X X <br /> X <br /> PROD.OIL X X <br /> CHLOR. X <br /> SOLVENTS X X <br /> NONCHLOR X <br /> SOLVENTS X X <br /> WASTE\ X X X X <br /> USED OIL X X X <br /> are <br /> All analysis methods are the designated EPA methods described in EPA SW 8endix D B 46,Third Edition. <br /> 1Table Those <br /> Soon page A20 for minimum detection <br /> specifically noted below. Refer to the "SWRCB LUFT Field Manual", App ( ) for Initial <br /> limits for motor vehicle fuel (gasoline and diesei)mmRefer <br /> mum det ct n lgimits.l Board Staff Detection Limits th teremain below the MCLuSTLC or <br /> Investigation of UST s for the waste and motor o <br /> Allowable Limit of the contaminant in question will be accepted,however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon,Gasoline,GC/FID(5030)8015 mod or GC/MS 8260 <br /> TPH-D Total Petroleum Hydrocarbon,Diesel,GCIFID(3550),8015 mod or GCMS 8260 <br /> BTX&EBenzene,Toluene,Xylene&Ethyl Benzene,GC/PID 8020 or GUMS 8260 <br /> CL HC Chlorinated Hydrocarbon,GC/HSD 8010,GC/MS 8240 or 8260 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or ICP-AES 6010 <br /> OXYGENATES MTBE,ETBE,TAME,DIPE,&TBA GC/MS 8260(For MTBE screen only you may use 8020) <br /> METALS ICAP or AA Inductively Coupled Plasma <br /> III and VI,Lead,Zinc and Nickel. 6010 or Atomic Absorption Spectrometry 7000. Metals: <br /> Cadmium,Chromium <br /> PCB Polychlorinated Biphenyls,GC/MS 8270 or 8080 <br /> GC-FID Gas Chromatography,Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> umns are <br /> ed to packed <br /> Notes: To avoid false positive detection of benzene,be samples s orsonce the hydrocarbons have been cholvents are to be used. Fused aracterized telriz d and properrQA/QC is followed.For <br /> packed column may be used as a"first "dirty" <br /> drinking water sources,EPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the detection <br /> limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination may require further analysis.PHS-EHD <br /> recommends holding those samples until disposal is indicated. <br /> EH 23 046 (Revised 05/09/00) <br /> 5 <br />