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Mr. Michael Walton <br />Walton Engineering <br />March 20, 1998 <br />LABORATORY ANALYSES AND RESULTS <br />All of the soil samples collected from beneath the former underground fuel storage tanks, fuel <br />dispenser islands, and underground product pipelines, and from the associated soil stockpile were <br />analyzed by California Laboratory Services, Inc., (CLS) of Rancho Cordova, California for: <br />• Total petroleum hydrocarbons in the range of gasoline (TPHg) using Environmental <br />Protection Agency (EPA) Method 8015 (modified) with purge and trap EPA Method 5030 <br />and/or <br />• Total petroleum hydrocarbons in the range of diesel fuel (TPHd) using EPA Method 8015 <br />(modified) with sonication EPA Method 3550 and <br />• Volatile organic compounds benzene, toluene, ethylbenzene, total xylene isomers (BTEX) <br />using EPA Method 8020 with purge and trap EPA Method 5030 <br />In addition to these analyses, the four soil samples collected from beneath former underground <br />storage tanks T1 and T2 and the four soil sample composites collected from the soil stockpiles were <br />analyzed for: <br />• Total lead using EPA Method 7421 <br />All of the soil samples collected from beneath the former underground storage tanks and from <br />beneath the former fuel dispenser islands were analyzed for: <br />• Volatile oxygenates di -isopropyl ether, ethyl t -butyl ether, methyl t -butyl ether, t -amyl <br />methyl ether, and t -butyl alcohol using EPA Method 8260 <br />Soil samples collected from the area of overexcavation and from beneath the abandoned product <br />P e <br />pipeline were analyzed for TPHg, TPHd and BTEX compounds using the aforementioned analytical <br />methods. CLS is accredited by the State of California to perform all of these analyses. <br />Laboratory results of soil samples collected from beneath the former underground storage tanks at <br />the site indicated that elevated concentrations of TPHg, TPHd, and BTEX compounds were detected <br />in the soil sample collected from beneath the northern end of storage tank Tl (T In on Table 1). Low <br />concentrations of TPHg and/or one or more of the BTEX compounds were detected in soil collected <br />from beneath the northern ends of the two fuel dispenser islands (FDI and FD2 on Table 1). <br />Detectable concentrations of TPHg, TPHd and BTEX compounds were not found in soil samples <br />collected from beneath any of the other underground storage tanks, fuel dispenser islands, or any of <br />the underground product delivery pipelines. Concentrations of total lead were not detected at or <br />greater than 10 parts per million (ppm) in any of the soil samples analyzed for total lead (Table 1). <br />The laboratory reports for these soil samples are presented in Appendix A <br />GRA YLAND ENVIRONMENTAL <br />Grayland 022-160.trr 4 <br />