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0 CLS Labs 0 <br />Analysis Report: Oxygenates by Capillary GC/MS, EPA Method 8260 <br />Client: Grayland Environmental <br />2731 Quail Street <br />Davis, CA 95616 <br />Project: <br />Date Sampled: 11/21/97 <br />Date Received: 11/21/97 <br />Date Extracted: 11/24/97 <br />Date Analyzed: 11/24/97 <br />Date Reported: 12/05/97 <br />Client ID No.: S-3-FD2 <br />Analyte <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />p-Bromoflucrobenzene <br />Analyte <br />Project No.: 022-160 <br />Contact: Jeff Clayton <br />Phone: (916)756-1441 <br />Lab Contact: George Hampton <br />Lab ID No.: P0595 -8A <br />Job No.: 810595 <br />COC Log No.: 32025 - 32024 <br />Batch No.: 21024 <br />Instrument ID: MS02 <br />Analyst ID: MARKW <br />Matrix: SOIL <br />SURROGATE <br />CAS No. <br />N/A <br />N/A <br />460-00-4 <br />Sample: S-3-FD2 <br />Results <br />CAS No. (ug/kg) <br />Surr Conc. <br />(ug/kg) <br />5000 <br />5000 <br />5000 <br />Surrogate <br />Recovery <br />(percent) <br />96 <br />110 <br />107 <br />Rep. Limit Dilution <br />(ug/kg) (factor) <br />Di -isopropyl ether <br />108-20-3 <br />ND <br />250 <br />50 <br />Ethyl Tertiary Butyl Ether <br />637-92-3 <br />ND <br />250 <br />50 <br />Methyl t -butyl ether <br />1634-04-4 <br />650 <br />250 <br />50 <br />Tertiary Amyl Methyl Ether <br />994-05-8 <br />ND <br />250 <br />50 <br />Tertiary Butyl Alcohol <br />75-65-0 <br />ND <br />5000 <br />50 <br />ND = Not detected at or above indicated Reporting Limit <br />CA DOHS ELAP Accreditation/Registration Number 1233 <br />3249 Fitzgerald Road Rancho Cordova, CA 95742 (916) 638-7301 Fax(916)638-4510 <br />