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1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />1 <br />0 CLS Labs 0 <br />Analysis Report: Oxygenates by Capillary GC/MS, EPA Method 8260 <br />Client: Grayland Environmental <br />2731 Quail Street <br />Davis, CA 95616 <br />Project: <br />Date Extracted: 11/25/97 <br />Date Analyzed: 12/02/97 <br />Date Reported: 12/05/97 <br />Project No.: 022-160 <br />Contact: Jeff Clayton <br />Phone: (916)756-1441 <br />Lab Contact: George Hampton <br />Lab ID No.: P0595 <br />Job No.: 810595 <br />COC Log No.: 32025 - 32024 <br />Batch No.: 21024 <br />Instrument ID: MS02 <br />Analyst ID: AMBERLEE <br />Matrix: SOIL <br />Analyte <br />MB SURROGATE <br />CAS No. <br />Surr Conc. <br />(ug/kg) <br />MB <br />Surrogate <br />Recovery <br />(percent) <br />Dibromofluoromethane <br />75-61-6 <br />50.0 <br />89 <br />Toluene -d8 <br />N/A <br />50.0 <br />88 <br />p-Bromofluorobenzene <br />460-00-4 <br />50.0 <br />88 <br />METHOD BLANK <br />Reporting <br />Results <br />Limit <br />Analyte <br />CAS No. <br />(ug/kg) <br />(ug/kg) <br />Tertiary Butyl Alcohol <br />75-65-0 <br />ND <br />100 <br />Methyl t -butyl ether <br />1634-04-4 <br />ND <br />5.0 <br />Di -isopropyl ether <br />108-20-3 <br />ND <br />5.0 <br />Ethyl Tertiary Butyl Ether <br />637-92-3 <br />ND <br />5.0 <br />Tertiary Amyl Methyl Ether <br />994-05-8 <br />ND <br />5.0 <br />ND = Not detected at or above indicated Reporting Limit <br />CA DOHS ELAP Accreditation/Registration Number 1233 <br />3249 Fitzgerald Road Rancho Cordova, CA 95742 (916) 638-7301 Fax(916)638-4510 <br />