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Analysis Report: Total Petroleum Hydrocarbons, EPA Method 8015 <br />Sonication, EPA Method 3550 <br />Client: Grayland Environmental <br />2731 Quail Street <br />Davis, CA 95616 <br />Project: <br />Date Extracted: 12/02/97 <br />Date Analyzed: 12/02/97 <br />Date Reported: 12/05/97 <br />Analyte <br />CAS No. <br />Project No.: 022-160 <br />Contact: Jeff Clayton <br />Phone: (916)756-1441 <br />Lab Contact: George Hampton <br />Lab ID No.: P0595A <br />Job No.: 810595 <br />COC Log No.: 32025 - 32024 <br />Batch No.: 21080 <br />Instrument ID: PGC06 <br />Analyst ID: SEPIDEHS <br />Matrix: SOIL <br />MATRIX SPIKE <br />MS Conc. <br />(mg/kg) <br />Diesel N/A 5.00 <br />MA = Recovery data is outside standard QC limits due to matrix <br />interference. LCS recovery data validates methodology. <br />MATRIX SPIKE DUPLICATE <br />Analyte <br />CAS No. <br />MSD Conc. <br />(mg/kg) <br />Diesel N/A 5.00 <br />MA = Recovery data is outside standard QC limits due to matrix <br />interference. LCS recovery data validates methodology. <br />RELATIVE % DIFFERENCE <br />Analyte <br />CAS No. <br />Diesel N/A <br />MA = Recovery data is outside standard QC limits due to matrix <br />interference. LCS recovery data validates methodology. <br />CA DOHS ELAP Accreditation/Registration Number 1233 <br />3249 Fitzgerald Road Rancho Cordova, CA 95742 (916) 638-7301 Fax (916) 638-4510 <br />MS <br />Recovery <br />(percent) <br />0 <br />MSD <br />Recovery <br />(percent) <br />MA <br />Relative <br />Percent <br />Difference <br />(percent) <br />