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MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> OXYGEN <br /> TANK TANK TPH-G TPH-D BTX&E CL HC TOTAL MTBE ATES NIVEAL PCB <br /> # CONTENTS 8013 8015 8020 8010 LEAD 8020 (MTBE. ICAP/ 8270 <br /> 8260 8260 8260 8240 7420 8260 TBA,DWE, AES or 8080 <br /> 8260 7421 ETBE, AA <br /> TAME) <br /> 8260 <br /> LEADED GAS X X X X <br /> UNLOAS X X X <br /> DIESEL X X <br /> KEROSENE X X X. <br /> UNK FUEL X X X X X <br /> PROD.OIL X X X <br /> CHLOR. X <br /> SOLVENTS X X <br /> NONCHLOR I <br /> SOLVENTS X X X <br /> WASTE\ <br /> USED OIL X X X X X X X <br /> mmmmj�MENNEENNOM I'll ummumusussugass Ammusu,, <br /> All analysis methods are the designated EPA methods described in EPA SW W,Third Edition, Those methods not found in SW 846 are <br /> specifically noted below. Refer to the"SwRcB LUFT Field Manuar,Appendix D(B),Table 3-5 on page A20 for minimum detection <br /> limits for or vehicle fiml (gasoline and diesel). Refer to "Tri-Regional Board Staff Recommendations for Initial Evaluation and <br /> Investigation of UST's"for the waste and motor oil minimum detection limits. Detection Limits that remain below the NIC"STLC or <br /> Allowable Limit of the contaminant in question will be accepted,however laboratory shall utillme the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon,Gasolme,G (5030)8015 mod or CTC/MS 8260 <br /> TPH-D Tom]Petroleum Hydrocarbon,Diesel,OCIFID(3550),8015 mod orGCfMS 8260 <br /> BTX&EBenzefy,- Toluene,Xylene&Ethyl Benz=c,00PID 8020 or GUMS 8260 <br /> CL HC Chlorinated Hydrocarbon,GC/HSD 8010,GC/MS 9240 or 8260 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or 1CP-AES 6010 <br /> OXYGENATES MTBE,ETRE,TAME,DIFE,&TBA (1011S 8260(For BE SEqgLonly you may use$020) <br /> METALS ICAP or AA Inductively CmVIed Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Metals; <br /> Cadmium,Chromium HI and VL Lead,Zinc and Nickel. <br /> PCB Polychiminated Biphenyls,GCIMS 8270 or 8080 <br /> GC-FID Gas ChrontatoWWhy,Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sampic preparation <br /> Method 3550 Sonication sample prqwation,extraction method <br /> Method 5030 Purge and trals sample preparUion <br /> QA/QC Quality Assumme,/Quality Control <br /> Notes: To avoid false positive detection of benzene,benzene-free solvents are to be used. Fused capillary columns are preferred to packed columns;a <br /> packed column my be used as a*first cut"with"dirty"samples or once the hydrocarbons have been chuacterized and proper QAIQC is followed. For <br /> drinking water sources,EPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the detection <br /> limits are lower and the QA/QC is better. Samples exhibiting any level of he metal contamination may require further analysis.PHS-ENI} <br /> recommends holding those samples until disposal is indicated. <br /> EH 23 046 (Revised 05/09M0) <br /> cl -d L;396*2629S 1-1031MOO2iUO WU20 :6 900a 12 qej <br />