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CASTLE ANALYTICAL LA ORATORY <br /> Environmental Testing Services 2333 Shuttle Drive, Atwater, CA 95301 Phone: (209) 384-2930 <br /> Certificate #2079 Fax: (209) 384-1507 <br /> BSK Laboratories Client Project ID: 9903000549 Sampled: 3-15-99 <br /> 1414 Stanislaus Street Reference Number: 2131 Received: 3-17-99 <br /> Fresno, CA 93706 Sample Description: Soil Extracted: 3-19-99 <br /> Attn: Sample Receiving Sample Prep/Analysis Method: EPA 5030/8015M, 8020 Analyzed: 3-19-99 <br /> Lab Numbers: 2131-1 S, 2S, 3S, 4S Reported: 3-19-99 <br /> TOTAL PETROLEUM HYDROCARBONS -GASOLINE <br /> WITH BTEX DISTINCTION <br /> ANALYTE REPORTING LIMIT SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br /> 103698 103699 103700 103701 <br /> NTP-3' NTP-6' NTP-9' New Pit 14' <br /> E/W Comp. E/W Comp. <br /> (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) <br /> BENZENE 0.0050 NO ND ND ND <br /> TOLUENE 0.0050 ND ND 0.010 NO <br /> ETHYL BENZENE 0.0050 ND ND ND NO <br /> TOTAL XYLENES 0.0050 ND ND 0.0074 NO <br /> GASOLINE RANGE 1.0 ND NO ND ND <br /> HYDROCARBONS <br /> Report Limit Multiplication Factor: 1 1 1 1 <br /> Surrogate % Recovery: FID-76.2%/PID-76.1% F10-88.7%/PID-88.8% FID-76.1%/PID-76.8% FID-91.7%/PID-92.0% <br /> Instrument ID: VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 <br /> Practical Quantitation Limit = Reporting Limit x Report Limit Multiplication Factor <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> ANALYST APPROVED BY: <br /> lari Cone Ja <br /> J. MW C p i lips <br /> Epvironmental Lab Director <br /> J <br />