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1 ll` i t 1/". t
<br />r u r•r r rr. r rr r•c r r'r t w :.;,, r , r • • r•r r• • wr
<br />MANY
<br />,;' •t u • rr•:♦ r t r' rs r :..,, .. . • .u•r,. :•.r• • sw' r'rw::
<br />Ilr rr rr r; r: rMr r.. r t r r' r r err : ra r: r r on De accep. -
<br />14owever laboratorythe most r ;'w method.
<br />TPH-G
<br />Total Petroleum Hydrocarbon, Gasoline, (5030) 8015 mod Or GC/MS 8260
<br />TPH-D
<br />Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260
<br />BTX & E
<br />TOTAL
<br />CL HC
<br />METALS
<br />TOTAL LEAD
<br />Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />EDB
<br />0302
<br />GC -FID
<br />Gas Chromatography, Flame Ionization Detection
<br />LEAD
<br />Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption
<br />ICAP/
<br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />PCB
<br />Polychlorinated Biphenyls, GCIMS 8270 Or 8080
<br />Method 3050
<br />Acid digestion
<br />Method 3540
<br />7420
<br />Method 3550
<br />AES or
<br />Method 5030
<br />Purge and trap sample preparation
<br />QA/QC
<br />Quality Assurance/Quality Control
<br />7421
<br />AA
<br />PROD. OIL—n
<br />MCHLOR.
<br />'I
<br />MMMMMEME
<br />i SOLVENTS
<br />M
<br />MMMMMEME
<br />SOLVENTS
<br />Mi�aaaa�■ae
<br />r u r•r r rr. r rr r•c r r'r t w :.;,, r , r • • r•r r• • wr
<br />MANY
<br />,;' •t u • rr•:♦ r t r' rs r :..,, .. . • .u•r,. :•.r• • sw' r'rw::
<br />Ilr rr rr r; r: rMr r.. r t r r' r r err : ra r: r r on De accep. -
<br />14owever laboratorythe most r ;'w method.
<br />TPH-G
<br />Total Petroleum Hydrocarbon, Gasoline, (5030) 8015 mod Or GC/MS 8260
<br />TPH-D
<br />Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260
<br />BTX & E
<br />Benzene, Toluene, Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 8260
<br />CL HC
<br />Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240
<br />TOTAL LEAD
<br />Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />EDB
<br />Ethylene dibromide (DHS -AB 1803), GC/MS 8240 (DHS-LUF1)
<br />GC -FID
<br />Gas Chromatography, Flame Ionization Detection
<br />ICAP or AA
<br />Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption
<br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />PCB
<br />Polychlorinated Biphenyls, GCIMS 8270 Or 8080
<br />Method 3050
<br />Acid digestion
<br />Method 3540
<br />Soxhlet sample preparation
<br />Method 3550
<br />Sonication sample preparation, extraction method
<br />Method 5030
<br />Purge and trap sample preparation
<br />QA/QC
<br />Quality Assurance/Quality Control
<br />Notes: To avoid Use positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns are
<br />preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons
<br />have been characterized and proper QA/AC is followed.
<br />For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600
<br />series because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal
<br />contamination may require further analysis. PHS-EHD recommends holding these samples until disposal is indicated.
<br />EH 23 048 (Revised 7/10/92) Page 8
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