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SAMPLING`i t i FOR ROUTINE it
<br />ISPENSER i
<br />The following represents minimum sampling criterion required for closure compliance. Soil samples collected shall be
<br />representative of native soils beneath the tank's invert (tank's bottom) at a collection depth not to exceed 2 - 4 feet. If
<br />contamination Is documented during closure, an Unauthorized Release Notification must be completed and submitted within five
<br />(5) working days pursuant to California Health & Safety Code, Section 25295.
<br />1. EPA Method 8260B analyses must include all analytes listed in the method plus fuel oxygenates methyl -
<br />tertiary -butyl ether (MTBE), diisopropyl ether (DIPE), ethyl -tertiary -butyl ether (EtBE), tertiary -amyl -methyl
<br />ether (TAME), tertiary -butanol (TBA), methanol and ethanol and fuel additives 1,2-dichioroethane (1,2 -DCA)
<br />and ethylene dibromide (EDB or 1,2-dibromoethane).
<br />2. If pentachlorophenol (PCP) is identified, analyze the soil and/or water sample for dioxins and furans by EPA
<br />Method 8290 and pesticides by EPA Method 8081A,
<br />3. METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption
<br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />4. Non-proprietary, performance based analytical methods may be used with approval of Regional Board staff.
<br />Revised 02/20/09
<br />utarCN=1K F'IL'ING AND STOCKPILE
<br />DISPENSER SAMPLES
<br />SAMPLES
<br />1 Sample beneath each dispenser
<br />PIPING SOIL SAMPLES
<br />1 Sample every 20 lineal feet
<br />DISPENSER & PIPING STOCKPILE SAMPLES
<br />2 Samples every 50 cubic yards
<br />1. EPA Method 8260B analyses must include all analytes listed in the method plus fuel oxygenates methyl -
<br />tertiary -butyl ether (MTBE), diisopropyl ether (DIPE), ethyl -tertiary -butyl ether (EtBE), tertiary -amyl -methyl
<br />ether (TAME), tertiary -butanol (TBA), methanol and ethanol and fuel additives 1,2-dichioroethane (1,2 -DCA)
<br />and ethylene dibromide (EDB or 1,2-dibromoethane).
<br />2. If pentachlorophenol (PCP) is identified, analyze the soil and/or water sample for dioxins and furans by EPA
<br />Method 8290 and pesticides by EPA Method 8081A,
<br />3. METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption
<br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />4. Non-proprietary, performance based analytical methods may be used with approval of Regional Board staff.
<br />Revised 02/20/09
<br />rUK
<br />UNuftRGROUND
<br />STORAGE
<br />TANK INVESTIGATIONS
<br />TANK
<br />##
<br />TANK
<br />CONTENTS
<br />TPN -G
<br />TPH-D
<br />BTX & E
<br />CL HC TOTAL MTBE
<br />OXYGENATES METALS PCB
<br />8015
<br />8015
<br />8020
<br />LEAD
<br />8010
<br />(MTBE, TBA, DIPS, ICAP/AES 827®
<br />8260
<br />8260
<br />8260
<br />8240 7420 8020
<br />ETBE,TAME) or 8080
<br />8260 7421 8260
<br />1,2 DCA & EDB AA
<br />8260
<br />LEADED GAS
<br />X
<br />X
<br />X
<br />X
<br />UNL GAS
<br />X
<br />X
<br />X
<br />DIESEL
<br />X
<br />X
<br />KEROSENE
<br />X
<br />X
<br />X
<br />UNK FUEL
<br />X
<br />X
<br />X
<br />X
<br />X
<br />PROD. OIL
<br />X
<br />X
<br />X
<br />CHLOR.
<br />SOLVENTS
<br />X
<br />X
<br />X
<br />NONCHLOR
<br />SOLVENTS
<br />X
<br />X
<br />X
<br />WASTEIUSED OIL
<br />OR
<br />UNKNOWN
<br />X
<br />X
<br />X
<br />X
<br />X
<br />X
<br />X
<br />CONTENTS
<br />Notes•
<br />1. EPA Method 8260B analyses must include all analytes listed in the method plus fuel oxygenates methyl -
<br />tertiary -butyl ether (MTBE), diisopropyl ether (DIPE), ethyl -tertiary -butyl ether (EtBE), tertiary -amyl -methyl
<br />ether (TAME), tertiary -butanol (TBA), methanol and ethanol and fuel additives 1,2-dichioroethane (1,2 -DCA)
<br />and ethylene dibromide (EDB or 1,2-dibromoethane).
<br />2. If pentachlorophenol (PCP) is identified, analyze the soil and/or water sample for dioxins and furans by EPA
<br />Method 8290 and pesticides by EPA Method 8081A,
<br />3. METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption
<br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />4. Non-proprietary, performance based analytical methods may be used with approval of Regional Board staff.
<br />Revised 02/20/09
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