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,/18/2005 09;01 20946 33 EHD PAGE 06 <br /> MINIMUM VERIFICATION LABORATORYANALYSIS <br /> TANK TANK TPH GTPH-D IM&E CL HC TOTAL MTBE OXYGEN <br /> ra CONTENTS 8013 80t5 ATES ►tarn6 <br /> 8010 8010 LEAD 8020 (tvtTBE, PCB <br /> 8260 8260 8260 8240 7420 8260 (MTBErt, .ICA P/ 8270 <br /> TBA82607421 ETBL, ALS or 8080 <br /> TAML AA <br /> 8 <br /> LEADED GAS X X <br /> X X <br /> UNL GAS X X <br /> DI ESE]. X X <br /> }( <br /> KEROSENE X X <br /> X <br /> UNK FUEL X X <br /> X X <br /> PROD.OIL X X <br /> X <br /> CHLOR. <br /> SOLVENT'S X X X <br /> NONCI-(LOR <br /> SOLVENTS X X X <br /> WASTE\ <br /> USED OIL X X X X <br /> All anatysla methods arc the designated EPA methods Described In EPA SW 846,Third Edition. 'I hose methods not found X SW 8 6 are <br /> specifically noted below, Refer to the "SWRCB LUFT Field Manual",Appendix D(B),Table 3-5 on Page A2 <br /> limits for motor vchlcic fuel (gasoline and diesel). Refer to "Tri-Rogiona) El <br /> D Staff R le 3-5 n Pagns for Initial Evaluation and <br /> P S 0 for minimum dctectton <br /> investigation of US'I"5" for the woute and motor oil minimum detection limits. Detectlou Limits that remain below the MCL,STLC or <br /> Allowxbic Limit or the eontat Alan(in question will be seeepted,however laboratory shall utilize the most conservative method. <br /> LABO <br /> TPH•G Tota)Pe tro)eum'tlydrocsrhot>, Gosolinc,GC/FID 50 0)8015 mod orTORYEGC/M 6TERMI00LOGY; <br /> TPFI•D Total Pctrolcum Hydrocarbon,Diesc.l,GC/FID(3550),8015 mod or GC/MS 8260 <br /> DTX& EBeruene,Toluene,Xylcne&Ethyl Benzine,GC/PM 8020 or GC/MS 8260 <br /> CL HC Chlorioatcd l lydroc ubon,GC/HSD 8010,GC/MS 8240 or 8260 <br /> TOTAL LEAD 1'oW)lead,AA J420, AA 7421 or ICP-AES 6010 <br /> OXYGENATES NnB8,ETBr;,TAME,DIPE,&TBA <br /> METALS tCAP ur AA GC/MS 8260(for MTBE r you may use 8020) <br /> Inductively Coupled Plasma Atomic EmisWon Spectrometry 6010 or Atomic Abs <br /> Cadmium,Chromium III and Vt,.Lead,Zinc and Nickel. orption Spectranetry 7000. MctAls: <br /> PCB Polychlorinatcd Biphenyls,GC/MS 8270 or 8080 <br /> GC-FID Gas Chromatography,Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> -Method 3540 SOXhIct sample Preparation <br /> hfeehod 3550 Sonication sample prepanxion,extraction method <br /> Method$030 Purge and trap sample preparation <br /> QA/QC Quality Asswunce/Quality Control <br /> Notes.' To avoid falsc positive dctccpon ofbenzenc,ben2enc-tier solvents arc to be used. Fused capii)aty columna ore preferred to pucked columns a <br /> packed cohinrn may be used m a"first cut"with"dirty"samples or ouce the hydrocarbons have been charactarized andProper A/ <br /> dru+kin8 water saarces,EPA rccommeiids that the 500$cries for volotile oryanic should be used in <br /> Q QC is followed. For <br /> lin its an lower and the se samples <br /> is butter. Samples c ndic ilcd any)evil of heavy metal cootaminadon may require further analysia.PHS-EHb <br /> preference to the 600$cries because the dctcctiun <br /> rrcorrunends holding those samples until disposal is indicated. <br /> 1H:3 046 (Reviicd 05/09!00) <br /> 5 <br />