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QC Sample Results <br /> Client: Hydro Analysis TestAmerica Job ID:720-49865-1 <br /> Project/Site:Tracy Blvd.,Valero <br /> Method: 8260B/CA LUFTMS -8260B/CA LUFT MS <br /> Lab Sample ID:MB 720-136932/4 Client Sample ID:Method Blank <br /> Matrix:Solid Prep Type:Total/NA <br /> Analysis Batch:136932 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Methyl tert-butyl ether ND 5.0 ug/Kg 05/22/13 20:25 1 <br /> Benzene ND 5.0 ug/Kg 05/22/13 20:25 1 <br /> Ethylbenzene ND 5.0 ug/Kg 05/22/13 20:25 1 <br /> Toluene ND 5.0 ug/Kg 05/22/13 20:25 1 <br /> Xylenes,Total ND 10 ug/Kg 05/22/13 20:25 1 <br /> Gasoline Range Organics(GRO) ND 250 ug/Kg 05/22/13 20:25 1 <br /> C5-C12 <br /> TBA ND 10 ug/Kg 05/22/13 20:25 1 <br /> DIPE ND 5.0 ug/Kg 05/22/13 20:25 1 <br /> TAME ND 5.0 ug/Kg 05/22/13 20:25 1 <br /> Ethyl t-butyl ether ND 5.0 ug/Kg 05/22/13 20:25 1 <br /> MB MB <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> 4-Bromo luorohenzene 67 45-131 05/22/13 20:25 1 <br /> 1,2-Dichloroethane-d4(Surr) 110 60-140 05/22/13 20:25 1 <br /> Toluene-d8(Surr) <br /> 78 58-140 05/22113 20:25 1 <br /> Lab Sample ID:LCS 720-136932/5 Client Sample ID:Lab Control Sample <br /> Matrix:Solid Prep Type:Total/NA <br /> Analysis Batch: 136932 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Methyl tert-butyl ether 50.0 51.1 ug/Kg 102 70-144 <br /> Benzene 50.0 50.8 ug/Kg 102 70-130 <br /> Ethylbenzene 50.0 54.9 ug/Kg 110 80-137 <br /> Toluene 50.0 53.2 ug/Kg 106 80-128 <br /> m-Xylene&p-Xylene 100 111 ug/Kg 111 70-146 <br /> o-Xylene 50.0 57.9 ug/Kg 116 70-140 <br /> TBA 1000 939 ug/Kg 94 63-130 <br /> DIPE 50.0 35.8 ug/Kg 72 70-131 <br /> TAME 50.0 55.7 ug/Kg 111 70-140 <br /> Ethyl t-butyl ether 50.0 45.0 ug/Kg 90 70-130 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromo luorobenzene 101 45-131 <br /> 1,2-Dichloroethane-d4(Surr) 102 60-140 <br /> Toluene-d8(Surr) 93 58-140 <br /> Lab Sample ID:LCS 720-136932/7 Client Sample ID: Lab Control Sample <br /> Matrix:Solid Prep Type:Total/NA <br /> Analysis Batch:136932 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Gasoline Range Organics(GRO) 1000 850 ug/Kg 85 61-128 <br /> -C5-C12 <br /> TestAmerica Pleasanton <br /> Page 11 of 24 5/23/2013 <br />