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MINIMUM VERIFICATION LABORATORY ANALYSIS 000151 <br /> TANK TAMC TPH-G TPH-D BTX& CL HC TOTAL EDB METALS PCR <br /> # CONTENTS 8015 8015 E 8010 LEAD [CAP/ 9270 <br /> 8200 8280 8021) 8240 7420 8250 AES or 9090 <br /> 92811 7421 AA <br /> LEADED GAS X X L X X <br /> LJNL GAS X X <br /> 838- DIESEL X X <br /> A''Z DIIJI <br /> KEROSENE X X <br /> UNK Fl TEL X X X X X <br /> PROD. OIL X X <br /> CHLOR. X X <br /> SOLVENTS <br /> NONCHLOR X X X <br /> SOLVEh?S <br /> WASTE\ X X X X X X <br /> I JSED OIL <br /> All analyses methods are designated EPA medi)ds described in EPA SW 846.Third Edition. Those medials not found in <br /> SW 848,are specifically noted below. Refer tothe"SWRCB LUFT Field Manual".Appendix A-20.Table 3-5 for detection <br /> limits of motor vehicle fuels(,asoline and diesel). Refer to 1-2-3"Regional Board Staff Recommendations for Initial <br /> Evaluation and Investigation of USTs" for the waste and moor oil detection limits. <br /> Detection Limits that remain below the MCL. STLC or Allowable Limit of the contaminant in <br /> question will he accepted, however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon.Gasoline.GC../FID(5030)8015 mod or GC/MS 8280 <br /> TPH-D Toucl Petroleum Hydrocarbon.Dicsel.GCIRD(3550).8015 mud or GC/MS 8260 <br /> BTX&E Benzene.l'oluene.Xylene:&Ethyl Benzene.GC/PM)8020 or GC/MS 8260 <br /> CL HC Chlimnated Hydrocarbon.G('/HSL)8010.GC/MS 8240 <br /> TOTAL LEAD Vaal lead.AA 7420. AA 7421 or ICP-AES 6010 <br /> U)B Ethylene dibromidc(DTSC-AB 1803).GC/MS 8240(DISC-LUFII <br /> (W-1711) (las Chro natography.Flame Ionization Detection <br /> I(:AP or AA Inductively coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Metals: Cadmium, Chromium Ill and VI. Lead, Zinc and Nickel. <br /> NCB Polycilorinated Biphenyls.GUMS 8270 or 8080 <br /> Method NN) Acid digestion <br /> MedmA 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation.extraction method <br /> Med"5030 Puree and trap sample prepwation <br /> QA/QC Quality Assurance/Quality Control <br /> Ncxes: To avoid false positive detection of benzene,benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns:a piKked column may be used as a"first cru"with"dirty"samples or once the hydrocarbons have <br /> been characterized and proper QA/AC is followed. <br /> For Dnnking water sources.EPA reconunends that the 50)series for volatile organics be used in preference to the 600 series <br /> because doe detection limits are lower and die QA/QC is better. Samples exhibiting any level of heavy metal contamination <br /> may require furd><v analysis. PHS-E11D recommends]holding dine samples until disposal is indicated. <br /> EH 23038(Rev 7/10192) <br /> x <br />