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MINIMUM VF,RIFICATION LABORATORY ANALYSIS •000086 <br /> TANK TANK TPH-(i TPH-D 13'IX& CL HC TOTAL E1113 I METALS PCB <br /> C )NIYNTS 9()15 X015 E x01() LEAD ICAP/ 8270 <br /> 8261) x261) x020 8240 7420 8240 AES or 8080 <br /> 8260 7421 AA <br /> LEADED(IAS x x x x <br /> UNL(IAS x X <br /> 805- DIESEL. X x <br /> Dll.rt <br /> KEROSENE- X X <br /> UNK FT TEL X X X X X <br /> PROD.OIL X X <br /> CHLOR. X X <br /> SOLVENTS <br /> NONCHLOR X X X <br /> SOLVENTS <br /> WASTE\ X X X X X X <br /> ITSED OIL, <br /> All analyses methods are designated EPA methods described in EPA SW 846,Third Edition. Those methods not found in <br /> SW 846,are specifically noted below. Refer to the"SWRCB LUFf Field Manual".Appendix A-20.'Fable 3-5 for detection <br /> limits of motor vehicle fuels(gasoline and diesel). Refer to 1-2-3"Regional Board Staff Recommendations for Initial <br /> Evaluation and Investigation of UST's" for the waste and motor oil detection limits. <br /> Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in <br /> question will he accepted, however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMWOLWY: <br /> TPH-Ci Total Petroleum Hydrocartwn.(rssoline.GC/FID(5030)8015 mai or(',C/MS 926() <br /> T PH-D Total Petroleum l Iydrocarbon.Diesel GC/FID(3550).8015 noxi or GUMS 8260 <br /> BTX&E Benzene,Toluene.Xylene&Ethyl Benzene.GC/PID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon.GC/HSD 8010.GC/MS 824() <br /> TOTAL LEAD Total lead.AA 7420. AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide(DISC-AB 1803).GC/MS 8240(DTSC-LUIT) <br /> GC-FID Gas Chnxtuuography.Flame Ionization Detection <br /> ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7(xx). Metals: Cadmium, Chromium IiI and VI, Lead, Zinc and Nickel. <br /> PCB Polychlorinated Biplienyls.GC/MS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3510 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of benzene,benzene-free solvents are to be used. Fused c..tpillary columns are <br /> preferred to packed columns;a pocked column may be used as a"first cut"with"dirty"samples or once tic hvdn)cartxrns have <br /> been characterized and proper QA/AC is followed. <br /> For Drinking water sources,EPA recommends that the 500 series for volatile organics be used in preference to the 61x)series <br /> because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination <br /> may require further analysis. PHS-EHD recommends holding these samples until disposal is indicated. <br /> EH 23 048(Rev 7/10/92) <br /> x <br />