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07/24/2006 12:59 4640138 ENVIRONMENTAL HEALTH PAGE 06 <br /> F` <br /> N MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> OXYGEN <br /> TANK TANK TPH-D BTX&F Cl.,HC: TOTAL MTBE ATES tr"AL PCB <br /> # CONTENTS 8415 8OT5 8020 8010 LEAF) 8420 TPAD ICRP/ 8270 <br /> 8260 8264 8260 8240 7420 6260 l ME� AES or 8090 <br /> 8260 7421 TAMP) AA <br /> B26tt <br /> LEADED GAS x EX X <br /> UNL OAS x X <br /> DIESEL, X <br /> KEROSENE x X x <br /> umK FUEL X x x x <br /> FRDD.OIL x x � <br /> CHLOR. X <br /> SOLVENTS x <br /> NONCHLOR X <br /> SOLVENTS x x <br /> WASTEt <br /> USM OIL x X x X x846 are <br /> X 7C <br /> All analysis methods are the designated EFA methods do saibed in EPA SW 846,Thirst Edit 0n. Those medKKb rot found in SW <br /> specifically noted below. Refer tai the"SWRC B LUFT Field Mortuat",AWMdix D(B`),Table 3y-5 can pagc A20 fvr rainimmn dztec6on <br /> limits for motor vehicle fuer (gasoline and diesel): Refer to "Tri-Regional Board Staff Recommendations fit' TnRW Evaluation and <br /> Investigation of U75"for the wwta and motor oil rniniat UM, detectiOn limits. Deftetim Uxtft that remain below the MCL,STL.0 or <br /> Atlowabk Limit at CMtWift2M in question will he a er jaboratM shah ttfitimae the most cowrvative method. <br /> LABORATORY ANAk.LYSP-5 TE L4CV: <br /> TPFT-G Total Petmimm 14ydrocwtor,Crssol'rnc,OC/RD(9030)8015 mod or GUMS 6260 <br /> TPN-D i oral T>chnieuru Hydrorban,Diesel;GCIFID(359#!) 8015 trod err GCJMS$260 <br /> RTX&E Benzene,Toluene,Xylem&Ethyl' (3071D$020 or GOMS 6260 <br /> Ci,HC Chlorinated Hydra D 8010,GC/MS 9240 or 8260 <br /> TUTA1.LEAD Total Mad,AA 742K AA 7421 or IC P-AFS 6010 <br /> QXYGENATES MTBE,ET-RE,TAMP_DIM&TBA GUMS 9260(For MTT tE se t you m"use 8020) <br /> METALS TCAP or AA Induct vety Coupled Plasma Atomic Emission Sptctremetry 6010 or Atomic Absorption Spectromcbj 7000. ls: <br /> Gadmitun,C—br*a Jum 1T1 sad V1,Lead,Zinc and Nickel'. <br /> PCB polycbla irtated Ri )s,OCM 9270 or 8480 <br /> GC-FID Gas Chrom y,Flame tern ixation Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhtet sample preparation <br /> Method 33550 Sonication sample preparation,cdrWicnt method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Hlssur®tn4e/(waltty Con"I <br /> _. a <br /> tllYifl3; <br /> Nolo: To avoid false positive detection of be<rzenc benzcns�fietivents arc tet be e�scd_ Fused capillary columns Are preferred Af Cis€oltowed. For <br /> packed column may be used as a"fust ctrl"with"dirty"samples or once,tf�trydrerbaus have been characterized and Proper Q Q <br /> drinking water sources.EPA recommends the detection <br /> that the 5 series for volatile orgataic sTatnztd he used p £rence to the anal sis PHS"E <br /> es <br /> limits arc lower and the QAfQC is better. Sam}ttes exhibking any fever of heavy metal coutamination map requim Y <br /> ffD <br /> recommends heckling those samples until dispersal is indicated- <br /> SH 23 046 (Revised 051D9W) <br /> 5 <br />