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f, <br /> MI IMUM VERlIFICATMON +133 `TORY ANALYSIS <br /> OXYGE I <br /> Ea rar. PCB <br /> TANX T TPiH-G TPH-D BTX&E CL HC LEADTOTA8020 (WfBF- ICRP/ 8270 <br /> CQ3�1'[ S 8015 8015 8020 8010 L TBA,DIPE. AES or 8080 <br /> 8260 8260 8260 8240 7420 8260 E.B� AA <br /> 8260 7421 TAME) <br /> 8260 <br /> LEADED GAS <br /> X X % <br /> X <br /> '[J1+IL GAS <br /> X <br /> DIESEL: X X <br /> X <br /> XX <br /> _ - X X <br /> X X <br /> X <br /> PROD.OIL X X <br /> CffljOk X <br /> ,OLE'EN S X X <br /> NON OR X <br /> SOLVENTS X X <br /> WASTES X X X <br /> USED OIL X X X <br /> tion. T1tQsn rr not o in SW$�16 are <br /> All clysis ods are the des' ed EPA me described in EPA SW$;Ifi, r,;nn S : are <br /> speci5eliy noted below_ fifer to the'°SWICB I: Field Manual",AppendixD(B),Table 3-5.ou page A20$c mi <br /> limits for rotor vehicle fuel (gasoline and.dieser. Refer to "Tri-l�eon <br /> �ic�a�al Board S Recommendations.fsrt tral Ev #ion and <br /> Li # <br /> Investigation of UST <br /> °°kir the waste 0"l rl,jaimum de#ection . Detection is thatremain below he MC <br /> `s L,STEL~or <br /> Allowable Limit of contaminant imm gves#inar w�be accep ,however laboratory shall the +as-t conservative method. <br /> LA-GP.ATORY ANALYSES'T NOLOGY: <br /> Tp,H-G 'T'otal Petroleum Hydrocarbon,Cramlinc,CURD(5030)$015 mod or GOMS 8260 <br /> Tpf1-D Total Pctroleum Hyrkocarbou,Diesel,GURD(3554).8015 mod of GCjMS$260 <br /> BTX&E Benzmc,Toluene,Xylene&Ethyl Benzene,CTUPfD 8020 or CONS 8260 <br /> CL HC Chlorinated-Hydrocarbon,GC/HSD 8010,GUMS 8240 or 8260 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or ICP-AES 5010 <br /> OXyGENATES MTBE,ETRE,TAME,RIPE,&'TBA WmS 8260(For Rel DE-Steen or ly you may use 8020) Speetrpm 7000. Metals:ME#AL:S;iCAP or,AA inductively Coupled Plasma Atomic Emission'Spectrometry 6010 or Atomic Absorption <br /> Cudemurta,Chrondudm 111 and Vii Lead,Zinc lad Nickel. <br /> PCS Polychlorinated Biphenyls,GOMS 8270 or 8080 <br /> --GG-Pla9 Cas Ghroma h 100ization Detection_ - <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample p "on,extraction method <br /> 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurdnoc/Quality Control <br /> Notes. To avoid false positive detection of benzene,�benznrae-free solvents are to be used. l°usi�capillary Columns ane prCfetted t�+packeds llowed�- For <br /> packed column may be used as a"first cut"with"dirty"samples or once the hydrocarbons have been characterized and pro pe Q <br /> drinking water sources,EPA rcco that the 500 series for volatile orf, jr,should be used in preference to the 600.scrie:s b the detection <br /> limits are lower and the QA/QC-is better. Samples exhibiting any level of heavy metal contamination'Tray require further analysis.PHS-END <br /> recd holding those samples until disposal is indicated. <br /> I <br /> EH 23 046 (Revised 05109/00) <br /> 9Gs ldH Hi-IV-gH "1t11N nMTAN-; BETS#9b ST:9T 9GOZ/EZ/EG <br />