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*Alpha Analytical, Inc. Sk <br /> ® 55 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: /� Work Order: <br /> 01-✓un-07 QC SuYY1111T1ata v Report 07052320 <br /> Method Blank Type MBLK Test Code:EPA Method SW8015B <br /> File ID:C:\HPCHEM\MS07\DATA\0705241 7052411.D Batch ID:MS07S7529B Analysis Date: 05/24/200711:13 <br /> Sample ID: MBLK MS07S7529B Units:pg/Kg Run ID:MSD_07 070524A Prep Date: 05/24/2007 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) NO 1000 <br /> Surr: 1,2-Dichloroethane-d4 164 200 82 69 126 <br /> Surr:Toluene-d8 198 200 99 80 120 <br /> Surr:4-Bromofluorobenzene 186 200 93 80 120 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8015B <br /> File ID:C:\HPCHEM\MS07\DATA\0705241 7052425.D Batch ID:MS07S7529B Analysis Date: 05/24/2007 17:00 <br /> Sample ID: GLCS MS07S7529B Units:pg/Kg Run ID:MSD 07 070524A Prep Date: 05/24/2007 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) 17900 2000 16000 112 58 141 <br /> Surr: 1,2-Dichloroethane-d4 320 400 80 69 126 <br /> Surr:Toluene-d8 373 400 93 80 120 <br /> Surr:4-Bromofluorobenzene 347 400 87 80 120 <br /> Sample Matrix Spike Type MS Test Code:EPA Method SW8015B <br /> File ID:C:\HPCHEM\MS07\DATA\070524\ 7052426.D Batch ID:MS07S7529B Analysis Date: 05/24/2007 17:22 <br /> Sample ID: 07052329-01AGS Units:pg/Kg Run ID:MSD_07_070524A Prep Date: 05/24/2007 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) 14800 2000 16000 0 93 46 142 <br /> Surr: 1,2-Dichloroethane-d4 303 400 76 69 126 <br /> Surr:Toluene-d8 393 400 98 80 120 <br /> Surr:4-Bromofluorobenzene 356 400 89 80 120 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8015B <br /> File ID:C:\HPCHEM\MS071DATA\0705241 7052427.D Batch ID:MS07S75296 Analysis Date: 05/24/200717:45 <br /> Sample ID: 07052329-01AGSD Units:pg/Kg Run ID:MSD_07 070524A Prep Date: 05/24/2007 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) 15700 2000 16000 0 98 46 142 14830 5.7(20) <br /> Surr: 1,2-Dichloroethane-d4 313 400 78 69 126 <br /> Surr:Toluene-d8 354 400 88 80 120 <br /> Surr:4-Bromofluorobenzene 364 400 91 80 120 <br /> Comments: <br /> Calculations are based off of raw(non-rounded data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> Reported in micrograms per kilogram,per clien request. <br />