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041pha Analytical, Inc. <br /> ® 55 Glendale Ave. -Suite 21 -Sparks,Nevada 89431-5778 <br /> (775)355-1044-(775)355-0406 FAX- 1-800-283-1183 <br /> Date: ®C SUmmary g�ep02t Work Order: <br /> 01-Jun-07 i� 07052320 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID:C:\HPCHEM1MS071DATA10705241 7052423.D Batch ID:MS07S7529A Analysis Date: 05/24/2007 16:14 <br /> Sample ID: 07052329-01AMS Units:pg/Kg Run ID:MSD 07 070524A Prep Date: 05/24/2007 <br /> Analyte Result PQL SpkVai SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> 1,1-Dichloroethene 192 20 400 0 48 21 160 <br /> Methyl tert-butyl ether(MTBE) 451 10 400 9.75 110 42 146 <br /> Benzene 472 10 400 0 118 57 140 <br /> Trichloroethene 474 20 400 0 119 58 139 <br /> Toluene 405 10 400 0 101 60 130 <br /> Chlorobenzene 418 20 400 0 104 61 130 <br /> Ethylbenzene 408 10 400 0 102 63 134 <br /> m,p-Xylene 411 10 400 0 103 64 136 <br /> o-Xylene 423 10 400 0 106 62 138 <br /> Surr:1,2-Dichlomethane-d4 318 400 80 69 126 <br /> Surr:Toluene-d8 379 400 95 80 120 <br /> Surr:4-Bromofluorobenzene 375 400 94 80 120 <br /> Sample Matrix Spike Duplicate Type MSD Test Code:EPA Method SW8260B <br /> File ID:C:\HPCHEMXMS071DATA\07052417052424.D Batch ID:MS07S7529A Analysis Date: 05/24/200716:37 <br /> Sample ID: 07052329-01AMSD Units:pg/Kg Run ID:MSD 07 070524A Prep Date: 05/24/2007 <br /> Analyte Result PQL SpkVai SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> 1,1-Dichloroethene 221 20 400 0 55 21 160 191.8 14.3(20) <br /> Methyl tert-butyl ether(MTBE) 431 10 400 9.75 105 42 146 451.3 4.7(20) <br /> Benzene 479 10 400 0 120 57 140 472 1.5(20) <br /> Trichloroethene 478 20 400 0 120 58 139 474.4 0.8(20) <br /> Toluene 404 10 400 0 101 60 130 404.7 0.1(20) <br /> Chlorobenzene 418 20 400 0 105 61 130 417.6 0.1(20) <br /> Ethylbenzene 408 10 400 0 102 63 134 408 0.0(20) <br /> m,p-Xylene 412 10 400 0 103 64 136 411.1 0.2(20) <br /> o-Xylene 420 10 400 0 105 62 138 423 0.6(20) <br /> Surr: 1,2-Dichloroethane-d4 305 400 76 69 126 <br /> Surr:Toluene-d8 387 400 97 80 120 <br /> Surr:4-Bromofluorobenzene 378 400 95 80 120 <br /> Comments: <br /> Calculations are based off of raw(non-rounded data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />