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1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> M c C a m b e 11 Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> t <br /> "When Quality Counts" http://www.mccanipbell.com/E-mail:main(a'mccampbell.com <br /> Analytical Report <br /> Client: Clean Harbors WorkOrder: 2006C77 <br /> Date Collected: 06/25/2020 13:00 Extraction Method: Polisini&Miller(CDFG 1988)(Haz.) <br /> Date Received: 06/25/2020 13:30 Analytical Method: Polisini&Miller(CDFG 1988)(Haz) <br /> Project: TOWER PARK Sample Matrix: Soil <br /> Hazardous Waste 96-hr Screening Bioassay w/ Fathead Minnows <br /> Lab ID _ 2006C77-001A S Sties Pime hales romelas Avg.Length(mm) 30.963 <br /> Client ID SAMPLE 1 Common Name Fathead Minnow Avg.Wei t 0.275698 <br /> Control Water Batch# EPASW 280 Organism Supplier ABS Max Weight 0.33456 <br /> Control Water Soft Synthetic Water Organism Log# 200626FHM Min Wei t 0.23004 <br /> Aux Control vH 8.50 Randomization N2 N/A Test Location TR2.2A <br /> Temperature(°C) pH D.O.(mg/L) EC(µS/cm) Survival <br /> Concentration Comments <br /> A B A B A B A B A B <br /> Control 19.7 19.7 7.60 7.60 9.0 9.0 163.0 162.5 10 10 Date: 6/27/2020 <br /> 250 mg/L 20.1 20.1 8.51 8.52 8.9 8.9 443.6 449.5 10 10 Time: 09:39 AM <br /> 500 mg/L 20.1 20.1 8.51 8.53 8.9 8.9 709.6 705.2 10 10 Analyst: CP <br /> 750 mg/L 20.1 20.2 8.54 8.53 8.9 8.9 936.4 970.9 10 LO Meter ID: MMO1 <br /> pH 8.5 Blk 20.1 20.1 8.53 8.50 8.9 8.9 196.4 196.4 10 10 <br /> Control 19.8 19.9 7.51 7.60 8.6 8.5 165.7 164.6 10 10 Date: 6/28/2020 <br /> 250 mg/L 20.1 20.0 7.97 8.02 8.4 8.3 476.8 483.9 10 10 Time: 09:46 AM <br /> 500 mg/L 20.1 20.1 8.10 8.15 8.3 8.1 740.7 747.4 10 L O Analyst: MAP <br /> 750 mg/L 20.2 20.2 8.19 8.25 8.2 8.2 974.8 1005 10 l0 Meter Ill: Mmol <br /> pH 8.5 Blk 20.2 20.3 7.84 7.72 8.6 M50 <br /> 197.3 10 10 <br /> Control 19.7 19.6 7.59 7.61 8.7 167.2 10 10 Date AT6/ 912020 280 mg/L 19.8 19.7 7.81 7.80 8.7 507.4 10 10 Time: 09 AM <br /> 800 mg/L 19.8 19.8 7.92 7.90 8.7 784.0 10 10 Analyst: MAP <br /> 750 mg/L 19.8 19.9 7.97 8.04 8.6 1054 10 10 Meter ID: MM02 <br /> pH 8.5 Blk 20.0 20.0 7.44 7.35 8.6 8.5 200.9 200.6 10 10 <br /> Control 19.7 19.6 7.44 7.43 8.8 8.8 170.8 169.4 10 10 Date: 6/30/2020 <br /> 250 mg/L 19.8 19.7 7.76 7.75 8.8 8.8 508.2 515.2 10 10 Time: 02:03 PM <br /> 500 mg/L 19.8 19.8 7.83 7.82 8.8 8.6 783.5 793.0 10 10 Analyst: ENM <br /> 750 mg/L 19.9 19.9 7.91 7.91 8.6 8.6 1033 1064 10 LO Meter ID: MM02 <br /> pH 8.5 Bik 20.0 20.0 7.37 7.34 8.9 8.8 202.4 202.3 10 l0 <br /> Control 19.7 19.4 7.62 7.33 8.7 8.7 172.8 171.6 10 to Date: 7/1/2020 <br /> 250 mg/L 19.8 19.7 7.60 7.70 8.8 8.9 511.9 520.9 lU 10 Time: 09:04 AM <br /> SOU mg/L 19.7 19.7 7.72 7.71 8.8 8.7 788.7 798.1 lU 10 Analyst: ENM <br /> 750 mg/L 19.8 19.8 7.79 7.78 8.7 8.7 1040 1070 10 10 Meter ID: MM02 <br /> pH 8.5 Blk 19.9 19.9 7.19 7.18 8.7 8.7 203.0 203.6 10 to <br /> initial Final <br /> Control 750 mg/L Control 750 mg/L <br /> Hardness(mg/L as CaCO3) 40 51 44 83 <br /> Alkalinity(mg/L as CaCO3) 33 88 34 105 <br /> Fish1D 1 2 3 4 5 6 . 8 9 0. <br /> Length(mm) 30.69 28.65 31.85 32.96 32.04 29.42 31.59 31.23 30.7 30.5 <br /> Weight(g) 0.29663 0.33456 0.25856 0.25732 0.31162 0.23004 0.24223 0.26109 0.23547 0.32946 <br /> Hazardous Waste Bioassay Sample Preparation Log <br /> Sample Prep Date Balance ID Sign-Off Date/Time On Shaker Sign-Off Date/Time On Shaker Sign-Off <br /> 6/26/2020 BL06 ENM 6/26/2020 1:35:00 PM I{AM 6/27/2020 8:00:00 AM CP <br /> (Cont.) <br /> CA ELAP 1644•NELAP 4033ORELAP <br /> n....,, c ..4 <br />