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i <br /> Report Number 31424 <br /> ANALYTICAL LLC Date 2/28/2003 <br /> Subject 6 Water Samples and 20 Soil Samples <br /> Protect Name BOYD SERVICE CENTER#4529 <br /> Project Number <br /> Case Narrative <br /> Hydrocarbons reported as'Bunker Oil'were quantitated against a motor oil standard <br /> Matrix Spike/Matnx Spike Duplicate Results associated with samples B-1 Water, B-2 Water, B-5 Water, <br /> *B-6 Water, B-4 Water for the analyte Methyl-t-butyl ether were affected by the analyte concentrations <br /> already present in the un-spiked sample Matrix Spike/Matnx Spike Duplicate Results associated with <br /> samples 8-5-4@21', B-6-3016', B-3-5@23 5'-24', 8-3-4@18 5'-19 51, 8-5-3@16', B-4-4.0_21', <br /> B-3-4@15 5-16 5, 8-3-3@16for the analyte Methyl-t-butyl ether were affected by the analyte <br /> concentrations already present in the un-spiked sample <br /> For sample B-4 Water, repeated analysis yielded inconsistent results for TPH as gasoline This should <br /> be considered an estimate due to the nature of the sample The result is flagged with a "J"to indicate that <br /> it is an estimate <br /> The Method Reporting Limit for TPM as Diesel has been increased due to the presence of <br /> high-boiling-range hydrocarbons for samples B-3-4@15 5-16 5, 8-3-4@18 5'-19 5', 8-4-2@11', <br /> 8-4-3@16', B-44021 , 8-5-3@16', B-3 Water and B-5 Water <br />