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Lancaster <br /> ! Laboratories Analysis Report <br /> 2425 New Holland Pike PO Bax 12425 Lancesier PA 176052425•717 6562300 Fax 717 656-2681•www lancaSterlabs corn <br /> Page 2 of 7 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 918531 <br /> Reported 11/11/04 at 06 35 PM <br /> Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL Unite %RSC %RBC Limits RPA APD Max <br /> N-Nitrosodiphenylamine N D 5 ug/1 94 74 63-104 23 30 <br /> 4-Bromophenyl-phenylether N D 5 ug/l 99 74 67-110 29 30 <br /> Hexachlorobenzene N D 10 ug/l 96 73 68-113 27 30 <br /> Phenanthrene N D 5 ug/1 93 76 68-111 19 30 <br /> Anthracene N D 5 ug/l 91 74 68-108 21 30 <br /> Di-n-butylphthalate N D 10 ug/1 69 71 63-113 22 30 <br /> Fluoranthene N D 5 ug/l 80 64* 66-108 23 30 <br /> Pyrene N D 5 ug/1 110 86 68-114 25 30 <br /> Butylbenzylphthalate N D 50 ug/1 103 80 63-120 25 30 <br /> Benzo(a)anthracene N D 5 ug/1 101 78 72-112 25 30 <br /> Chrysene N D 5 ug/1 102 79 70-111 25 30 <br /> 3,31-D2chlorobenzidine N D 10 ug/l 92 74 37-117 22 30 <br /> bis(2-Ethylhexyl)phthalate N D 10 ug/1 107 85 62-126 22 30 <br /> Di-n-octylphthalate N D 10 ug/l 117 89 58-118 27 30 <br /> Benzo(b)fluoranthene N D 5 ug/1 110 86 67-117 24 30 <br /> Senzo(k)fluoranthene N D 5 ug/l 111 87 67-120 24 30 <br /> Benzo(a)pyrene N D 5 u9/1 104 66 68-121 19 30 <br /> Indeno(1,2,3-cd)pyrene N D 10 ug/1 112 90 67-122 22 30 <br /> Dibenz(a,h)anthracene N D 10 u9/1 116 92 71-129 24 30 <br /> Benzo(g,h,i)perylene N D 5 ug/l 115 90 67-121 24 30 <br /> 2-Methylphenol N D 5 ug/l 80 62 56-105 26 30 <br /> 4-Methylphenol N D 5 ug/1 73 57 51-98 25 30 <br /> Benzyl alcohol N D 5 ug/l 78 67 54-100 16 30 <br /> Benzoic acid N D 10 ug/l 46 47 6-73 0 30 <br /> Batch number 04306112601A Sample number(s) 4391329 <br /> TRPH 418 1 N D 0 40 mg/l 81 63 54-113 3 14 <br /> Batch number 04307A53A Sample number(s) 4391328-4391329,4391331-4391332 <br /> TPH-GRO - Waters N D 50 ug/l 101 100 70-130 2 30 <br /> Batch number 04307A53B Sample number(s) 4391333 <br /> TPH-GRO - Waters N D 50 u9/1 101 100 70-130 2 30 <br /> Batch number 043080015A Sample number(s) 4391329,4391331-4391333 <br /> TPH-DRO CALUFT(Waters) N D 50 ug/1 81 86 61-126 6 20 <br /> Batch number 043101848001 Sample number(a) 4391330 <br /> Cadmium N D 0 00076 mg/l 98 97-111 <br /> Chromium N D 0 0025 mg/l 98 95-112 <br /> Lead N D 0 0100 mg/l 99 93-110 <br /> Nickel N D 0 0031 mg/l 99 93-110 <br /> Zinc N D 0 0048 mg/l 99 94-112 <br /> Batch number N043061AA Sample number(s) 4391329 <br /> Ethanol N D 500 u9/1 109 46-145 <br /> Methyl Tertiary Butyl Ether N D 2 u9/1 101 77-127 <br /> di-Isopropyl ether N D 2 ug/l 126 67-130 <br /> Ethyl t-butyl ether N D 2 ug/l 102 74-120 <br /> t-Amyl methyl ether N D 2 ug/l 94 79-113 <br /> t-Butyl alcohol N D 100 ug/l 91 57-141 <br /> Dichlorodifluoromethane N D 2 u9/1 135 53-184 <br /> Chloromethane N D 2 u9/1 140 66-143 <br /> vinyl Chloride N D 1 ug/l 117 71-134 <br /> Bromomethane N D 2 ug/l 105 55-131 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> . (2) The background result was more than four times the spike added <br />